Triethyl Orthoformate-d1

Base Information

• Chemical Name: Triethyl Orthoformate-d1
• CAS No.: 26387-53-1
• Molecular Formula: DC(OCH2CH3)3
• Molecular Weight: 149.194
• Mol file: 26387-53-1.mol

Synonyms:triethoxy<2H1>methane;deuterio-triethoxy-methane;Triethoxy-<2-ethylenimino-ethyl>-silan;C-deuterio-orthoformic acid triethyl ester;triethoxydeuteromethane;triethyl orthoformate-D;1,1,1-triethoxy-1-deuteromethane;

Chemical Property of Triethyl Orthoformate-d1

Chemical Property:

• PSA: 27.69000
• LogP: 1.37950

Purity/Quality:

99%, ^*data from raw suppliers

TriethylOrthoformate-d1 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Triethyl Orthoformate-d1

There total 2 articles about Triethyl Orthoformate-d1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

chloroform-d1 (865-49-6) + ethyl [2]alcohol (925-93-9) → [diethoxy(2H)methoxy]ethane (26387-53-1)

Guidance literature:

With sodium; Cooling with ice;

DOI:10.1039/b913399b

Reference yield:

→ [diethoxy(2H)methoxy]ethane (26387-53-1)

Guidance literature:

deuteriertes Formimino-ethylester-deuteriochlorid, 1) wasserfr. EtOH, Raumtemp., 2) Rk.-Gemisch, Ether, Siedetemp.;

DOI:10.1016/S0040-4020(01)93230-2

Reference yield: 87.0%

cycl-isopropylidene malonate (2033-24-1) + [diethoxy(2H)methoxy]ethane (26387-53-1) + aniline (62-53-3) → 2,2-dimethyl-5-((phenylamino)(2H)methylene)-1,3-dioxane-4,6-dione

Guidance literature:

In ethanol; for 1.5h; Reflux;

upstream raw materials:

chloroform-d1

ethyl [2]alcohol

Downstream raw materials:

ethyl deuterioformate

tert-butyl alcohol

Diethyl carbonate

3-deuterio-3,3-diethoxy-1-(phenylseleno)-1-propyne