2-(BOC-Amino)-4-methylphenylboronic acid,pinacol

Base Information

Chemical Name:2-(BOC-Amino)-4-methylphenylboronic acid,pinacol
CAS No.:1150561-75-3
Molecular Formula:C18H28BNO4
Molecular Weight:333.236
Hs Code.:2934999090
Mol file:1150561-75-3.mol

Synonyms:2-(BOC-AMINO)-4-METHYLPHENYLBORONIC ACID;2-(BOC-Amino)-4-methylphenylboronic acid,pinacol;tert-Butyl (5-Methyl-2-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbaMate;Carbamic acid, N-[5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]-, 1,1-dimethylethyl ester

Suppliers and Price of 2-(BOC-Amino)-4-methylphenylboronic acid,pinacol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(tert-Butoxycarbonylamino)-4-methylphenylboronic acid pinacol ester
100mg
$ 130.00

TRC
2-(tert-Butoxycarbonylamino)-4-methylphenylboronic acid pinacol ester
10mg
$ 45.00

Sigma-Aldrich
2-(tert-Butoxycarbonylamino)-4-methylphenylboronic acid pinacol ester Aldrich
1g
$ 249.00

Crysdot
tert-Butyl(5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbamate 95+%
5g
$ 856.00

American Custom Chemicals Corporation
2-(BOC-AMINO)-4-METHYLPHENYLBORONIC ACID, PINACOL ESTER 95.00%
5G
$ 1674.81

Alichem
tert-Butyl(5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbamate
1g
$ 400.00

Total 3 raw suppliers

Chemical Property of 2-(BOC-Amino)-4-methylphenylboronic acid,pinacol

Chemical Property:

PSA：56.79000
LogP:3.71420
Storage Temp.:2-8°C

Purity/Quality:

95%-98% ^*data from raw suppliers

2-(tert-Butoxycarbonylamino)-4-methylphenylboronic acid pinacol ester ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(BOC-Amino)-4-methylphenylboronic acid,pinacol

There total 4 articles about 2-(BOC-Amino)-4-methylphenylboronic acid,pinacol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1186637-29-5
tert-butyl (2-bromo-5-methylphenyl)carbamate

: 73183-34-3
bis(pinacol)diborane

: 1150561-75-3
tert-butyl 5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenylcarbamate

Guidance literature:: With sodium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 100 ℃; Inert atmosphere;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1150561-75-3
tert-butyl 5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

1.2: 20 °C

2.1: sodium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 100 °C / Inert atmosphere

With sodium acetate; sodium hexamethyldisilazane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane;

Reference yield:

: 53078-85-6
2-bromo-5-methylaniline

: 1150561-75-3
tert-butyl 5-methyl-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

1.2: 20 °C

2.1: sodium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 100 °C / Inert atmosphere

With sodium acetate; sodium hexamethyldisilazane; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane;