Benzamide, 2-amino-3-bromo-

Base Information

• Chemical Name: Benzamide, 2-amino-3-bromo-
• CAS No.: 437998-34-0
• Molecular Formula: C7H7BrN2O
• Molecular Weight: 215.049
• Hs Code.: 2924299090
• Mol file: 437998-34-0.mol

Synonyms:BenzaMide, 2-aMino-3-broMo-

Chemical Property of Benzamide, 2-amino-3-bromo-

Chemical Property:

• Melting Point: 249-250 °C
• Boiling Point: 292 ºC
• PKA: 15.15±0.50(Predicted)
• Flash Point: 131 ºC
• PSA: 70.10000
• Density: 1.698
• LogP: 2.59560
• Storage Temp.: Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

2-Amino-3-bromobenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzamide, 2-amino-3-bromo-

There total 3 articles about Benzamide, 2-amino-3-bromo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

2-amino-3-bromo benzoic acid (20776-51-6) → 2-amino-3-bromobenzamide (437998-34-0)

Guidance literature:

With ammonium chloride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 6h; Inert atmosphere;

Reference yield: 76.0%

7-bromoisatin (20780-74-9) → 2-amino-3-bromobenzamide (437998-34-0)

Guidance literature:

With ammonium hydroxide; dihydrogen peroxide; In dimethyl sulfoxide; at 20 - 30 ℃; Sealed tube;

DOI:10.1016/j.tet.2019.01.067

Reference yield:

8-bromo-1H-benzo[d][1,3]oxazine-2,4-dione (331646-98-1) → 2-amino-3-bromobenzamide (437998-34-0)

Guidance literature:

With ammonium carbonate; In 1,4-dioxane; at 60 ℃;

DOI:10.1021/acs.jafc.5b01762

upstream raw materials:

2-amino-3-bromo benzoic acid

8-bromo-1H-benzo[d][1,3]oxazine-2,4-dione

7-bromoisatin

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