Bicyclo[2.2.1]heptane, 2,3-dichloro-, (endo,endo)- (9CI)

Base Information

• Chemical Name: Bicyclo[2.2.1]heptane, 2,3-dichloro-, (endo,endo)- (9CI)
• CAS No.: 89577-09-3
• Molecular Formula: C7H10Cl2
• Molecular Weight: 165.0603
• Hs Code.: 2903890090
• Mol file: 89577-09-3.mol

Synonyms:Bicyclo[2.2.1]heptane, 2,3-dichloro-, (endo,endo)- (9CI)

Chemical Property of Bicyclo[2.2.1]heptane, 2,3-dichloro-, (endo,endo)- (9CI)

Chemical Property:

• PSA: 0.00000
• LogP: 2.63110

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.1]heptane, 2,3-dichloro-, (endo,endo)- (9CI)

There total 9 articles about Bicyclo[2.2.1]heptane, 2,3-dichloro-, (endo,endo)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

norborn-2-ene (498-66-8) + acetic anhydride (108-24-7) → trans-2,3-Dichlornorbornan (2843-43-8,14627-75-9,89577-09-3,101011-90-9) + endo-2,endo-3-dichloronorbornane (14627-75-9) + trans-2-Acetoxy-3-chloronorbornane (93955-44-3)

Guidance literature:

With Nitryl chloride;

Reference yield: 19.0%

norborn-2-ene (498-66-8) → trans-2,3-Dichlornorbornan (2843-43-8,14627-75-9,89577-09-3,101011-90-9) + endo-2,endo-3-dichloronorbornane (14627-75-9)

Guidance literature:

With Mn(IV)(N,N'-disalicylidene-1,3-diaminopropane^(2-))Cl₂; In dichloromethane; at 20 ℃;

DOI:10.1039/c39950002015

Reference yield:

→ trans-2,3-Dichlornorbornan (2843-43-8,14627-75-9,89577-09-3,101011-90-9)

Guidance literature:

With ethyl acetate; platinum;

DOI:10.1021/ja01651a027

upstream raw materials:

1,2-Dichlorethylen-cyclopentadien-Addukt

cyclopenta-1,3-diene

norborn-2-ene

norbornene

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