2,4-Dichloro-alpha-(chloromethyl)benzenemethanol methanesulfonate

Base Information

Chemical Name:2,4-Dichloro-alpha-(chloromethyl)benzenemethanol methanesulfonate
CAS No.:53984-39-7
Molecular Formula:C9H9Cl3O3S
Molecular Weight:303.594
Hs Code.:
Mol file:53984-39-7.mol

Synonyms:2-Chloro-1-(2,4-dichlorophenyl)ethyl methanesulfonate;2,4-Dichloro-α-(chloromethyl)benzenemethanol methanesulfonate;2,4-Dichloro-alpha-(chloromethyl)benzenemethanol methanesulfonate;Benzenemethanol, 2,4-dichloro-α-(chloromethyl)-, 1-methanesulfonate

Suppliers and Price of 2,4-Dichloro-alpha-(chloromethyl)benzenemethanol methanesulfonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-Chloro-1-(2,4-dichlorophenyl)ethylmethanesulfonate 97%
10g
$ 500.00

Crysdot
2-Chloro-1-(2,4-dichlorophenyl)ethylmethanesulfonate 97%
5g
$ 300.00

Crysdot
2-Chloro-1-(2,4-dichlorophenyl)ethylmethanesulfonate 97%
1g
$ 100.00

Total 20 raw suppliers

Chemical Property of 2,4-Dichloro-alpha-(chloromethyl)benzenemethanol methanesulfonate

Chemical Property:

PSA：51.75000
LogP:4.33030

Purity/Quality:

99% ^*data from raw suppliers

2-Chloro-1-(2,4-dichlorophenyl)ethylmethanesulfonate 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,4-Dichloro-alpha-(chloromethyl)benzenemethanol methanesulfonate

There total 3 articles about 2,4-Dichloro-alpha-(chloromethyl)benzenemethanol methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 13692-14-3,114446-57-0
α-(chloromethyl)-2,4-dichlorobenzyl alcohol

: 124-63-0
methanesulfonyl chloride

: 53984-39-7,229334-55-8
[2-chloro-1-(2,4-dichlorophenyl)ethyl] methanesulfonate

Guidance literature:: With triethylamine; In ethyl acetate; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1055/s-0037-1610341

Reference yield:

: 4252-78-2
2,2',4'-trichloroacetophenone

: 53984-39-7,229334-55-8
[2-chloro-1-(2,4-dichlorophenyl)ethyl] methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium tetrahydroborate / 0.25 h / 0 °C

2: triethylamine / ethyl acetate / 0.17 h / 0 °C

With methanol; sodium tetrahydroborate; triethylamine; In ethyl acetate;