AKOS BC-0240

Base Information

• Chemical Name: AKOS BC-0240
• CAS No.: 78056-28-7
• Molecular Formula: C11H19N
• Molecular Weight: 165.279
• Hs Code.: 2921300090
• Mol file: 78056-28-7.mol

Synonyms:1-Amino-3-methyladamantane;

Chemical Property of AKOS BC-0240

Chemical Property:

• Boiling Point: 232.206 °C at 760 mmHg
• PKA: 10.78±0.40(Predicted)
• Flash Point: 93.343 °C
• PSA: 26.02000
• Density: 1.056 g/cm³
• LogP: 3.00430

Purity/Quality:

99% ^*data from raw suppliers

1-Amino-3-methyladamantane 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of AKOS BC-0240

There total 5 articles about AKOS BC-0240 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-acetamido-3-methyltricyclo[3.3.1.13,7]decane (778-09-6) → 3-methyl-1-aminoadamantane (78056-28-7)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/jm00342a029

Reference yield:

1-bromo-3-methyladamantane (702-77-2) → 3-methyl-1-aminoadamantane (78056-28-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / Heating

2: NaOH / bis-(2-hydroxy-ethyl) ether / Heating

With sodium hydroxide; In diethylene glycol;

DOI:10.1021/jm00343a010

Reference yield:

3-methyl-1-adamantanol (702-81-8) → 3-methyl-1-aminoadamantane (78056-28-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 85 percent / Ph₃P, Br₂ / acetonitrile / 30 h / Heating

2: 78 percent / Heating

3: NaOH / bis-(2-hydroxy-ethyl) ether / Heating

With sodium hydroxide; bromine; triphenylphosphine; In acetonitrile; diethylene glycol;

DOI:10.1021/jm00343a010

upstream raw materials:

1-acetamido-3-methyltricyclo[3.3.1.1^3,7]decane

1-bromo-3-methyladamantane

3-methyl-1-adamantanol

1-methyl-adamantane

Downstream raw materials:

N'--N-<3-methyl-adamantyl>-harnstoff