2-(1,6,7,8-Tetrahydro-2H-indeno[5,4-b]furan-8-yl)ethylamine hydrochloride

Base Information

• Chemical Name: 2-(1,6,7,8-Tetrahydro-2H-indeno[5,4-b]furan-8-yl)ethylamine hydrochloride
• CAS No.: 1053239-39-6
• Molecular Formula: C13H18ClNO
• Molecular Weight: 239.745
• Mol file: 1053239-39-6.mol

Synonyms:2-(1,6,7,8-Tetrahydro-2H-indeno[5,4-b]furan-8-yl)ethylaMine hydrochloride; 1,6,7,8-Tetrahydro-2H-Indeno[5,4-B]Furan-8-Ethanamine Hydrochloride

Chemical Property of 2-(1,6,7,8-Tetrahydro-2H-indeno[5,4-b]furan-8-yl)ethylamine hydrochloride

Chemical Property:

• Melting Point: 165-167℃
• PSA: 35.25000
• Density: 1.058±0.06 g/cm3 (20oC 760 Torr)
• LogP: 3.50240

Purity/Quality:

99%, ^*data from raw suppliers

2-(2,6,7,8-Tetrahydro-1H-indeno[5,4-b]furan-8-yl)ethanamineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(1,6,7,8-Tetrahydro-2H-indeno[5,4-b]furan-8-yl)ethylamine hydrochloride

There total 6 articles about 2-(1,6,7,8-Tetrahydro-2H-indeno[5,4-b]furan-8-yl)ethylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2-(1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)acetonitrile (221530-44-5) → 2?(1,6,7,8?tetrahydro?2H?indeno[5,4?b]furan?8?yl)ethylamine hydrochloride (1053239-39-6)

Guidance literature:

With hydrogen; platinum(IV) chloride; In methanol; chloroform; at 30 - 40 ℃; for 2h; under 2250.23 - 3750.38 Torr; Solvent; Reagent/catalyst;

Reference yield: 87.0%

(2E)-2-(4,5-dibromo-1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)ethanamine hydrochloride → 2?(1,6,7,8?tetrahydro?2H?indeno[5,4?b]furan?8?yl)ethylamine hydrochloride (1053239-39-6)

Guidance literature:

(2E)-2-(4,5-dibromo-1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)ethanamine hydrochloride; With sodium carbonate; In water; toluene;

With hydrogen; sodium acetate; palladium 10% on activated carbon; In methanol; toluene; at 50 ℃; under 3310.08 Torr;

With hydrogenchloride; In isopropyl alcohol; toluene; at 30 ℃; for 2h; pH=2;

Reference yield:

C13H15NO2 (1053239-38-5) → 2?(1,6,7,8?tetrahydro?2H?indeno[5,4?b]furan?8?yl)ethylamine hydrochloride (1053239-39-6)

Guidance literature:

C₁₃H₁₅NO₂; With sodium tetrahydroborate; boron trifluoride diethyl etherate; In tetrahydrofuran; at 25 - 35 ℃; for 24 - 25h;

With hydrogenchloride; In water; ethyl acetate;

upstream raw materials:

C₁₃H₁₅NO₂

1,2,6,7-tetrahydro-8H-indeno[5,4-b]-furan-8-one

2-(1,2,6,7-tetrahydro-8H-indeno[5,4-b]furan-8-ylidene)acetonitrile

Downstream raw materials:

N-[2-(1,6,7,8-tetrahydro-2H-indeno[5,4-b]furan-8-yl)ethyl]propionamide

2?(1,6,7,8?tetrahydro?2H?indeno[5,4?b]furan?8?yl)?1?ethylamine

ramelteon

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