2,5-DIBROMOBENZENE ACETONITRILE

Base Information

• Chemical Name: 2,5-DIBROMOBENZENE ACETONITRILE
• CAS No.: 74533-21-4
• Molecular Formula: C8H5Br2N
• Molecular Weight: 274.942
• Hs Code.: 2926909090
• Mol file: 74533-21-4.mol

Synonyms:2,5-DIBROMOBENZENE ACETONITRILE;2-(2,5-dibroMophenyl)acetonitrile;2,5-Dibromophenylacetonitrile

Chemical Property of 2,5-DIBROMOBENZENE ACETONITRILE

Chemical Property:

• Vapor Pressure: 9.5E-05mmHg at 25°C
• Boiling Point: 338.9°C at 760 mmHg
• Flash Point: 158.8°C
• PSA: 23.79000
• Density: 1.857g/cm³
• LogP: 3.27768
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

2-(2,5-Dibromophenyl)acetonitrile 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,5-DIBROMOBENZENE ACETONITRILE

There total 6 articles about 2,5-DIBROMOBENZENE ACETONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

1,4-dibromo-2-(bromomethyl)benzene (136105-40-3) → 2-(2,5-dibromophenyl)acetonitrile (74533-21-4)

Guidance literature:

In dimethyl sulfoxide; at 50 - 90 ℃; for 0.333333h;

DOI:10.1055/s-0030-1260328

Reference yield: 82.0%

2,5-dibromobenzyl chloride (642091-49-4) → 2-(2,5-dibromophenyl)acetonitrile (74533-21-4)

Guidance literature:

With copper(I) cyanide; In N,N-dimethyl-formamide; at 125 - 130 ℃; Reagent/catalyst;

Reference yield: 50.0%

potassium cyanide (151-50-8) + 2,5-dibromobenzyl chloride (642091-49-4) → 2-(2,5-dibromophenyl)acetonitrile (74533-21-4)

Guidance literature:

In dimethyl sulfoxide; at 20 ℃; for 24h;

DOI:10.1021/jm060199b

upstream raw materials:

potassium cyanide

2,5-dibromobenzyl chloride

2,5-dibromobenzoic acid

(2,5-dibromophenyl)methanol

Downstream raw materials:

2-(2,5-dibromophenyl)-acetic acid

2-(2,5-dibromophenyl)-N-methoxyacetamide

(2,5-dibromo-phenyl)-acetyl chloride

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