Benzaldehyde, 3-fluoro-4-(4-methyl-1H-imidazol-1-yl)-

Base Information

• Chemical Name: Benzaldehyde, 3-fluoro-4-(4-methyl-1H-imidazol-1-yl)-
• CAS No.: 937400-07-2
• Molecular Formula: C11H9FN2O
• Molecular Weight: 204.204
• Hs Code.: 2933299090
• Mol file: 937400-07-2.mol

Synonyms:3-Fluor-4-(4-methyl-1H-imidazol-1-yl)benzaldehyd; 3-fluoro-4-(4-methyl-1H-imidazol-1-yl)benzaldehyde

Chemical Property of Benzaldehyde, 3-fluoro-4-(4-methyl-1H-imidazol-1-yl)-

Chemical Property:

• Vapor Pressure: 1.98E-05mmHg at 25°C
• Boiling Point: 362.1°C at 760 mmHg
• Flash Point: 172.8°C
• PSA: 34.89000
• Density: 1.21g/cm³
• LogP: 2.13230
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

3-Fluoro-4-(4-methyl-1H-imidazol-1-yl)benzaldehyde 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzaldehyde, 3-fluoro-4-(4-methyl-1H-imidazol-1-yl)-

There total 2 articles about Benzaldehyde, 3-fluoro-4-(4-methyl-1H-imidazol-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

4-methyl-1H-imidazole (822-36-6) + 3,4 difluorobenzaldehyde (34036-07-2) → 3-fluoro-4-(4-methyl-1H-imidazol-1-yl)benzaldehyde (937400-07-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 18h; Inert atmosphere;

Reference yield:

4-methyl-1H-imidazole (822-36-6) + 3,4 difluorobenzaldehyde (34036-07-2) → 3-fluoro-4-(4-methyl-1H-imidazol-1-yl)benzaldehyde (937400-07-2) + 3-fluoro-4-(5-methyl-1H-imidazol-1-yl)benzaldehyde (1415565-05-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃;

Reference yield:

3-fluoro-4-(4-methyl-1H-imidazol-1-yl)benzaldehyde (937400-07-2) → (Z)-(S)-2-[1-[3-fluoro-4-(4-methyl-1H-imidazol-1-yl)phenyl]methylidene]-4-[(1R,2R)-2-hydroxy-1-(3,4,5-trifluorophenyl)propyl]-6-methylmorpholin-3-one (937398-67-9)

Guidance literature:

(S)-4-[(1R,2R)-2-(tert-butyl-diphenyl-silanyloxy)-1-(3,4,5-trifluorophenyl)propyl]-2-hydroxy-6-methylmorpholin-3-one; With triphenylphosphine hydrobromide; In acetonitrile; for 1h; Heating / reflux;

3-fluoro-4-(4-methyl-1H-imidazol-1-yl)benzaldehyde; With triethylamine; In ethanol; at 20 ℃; for 1h;

With sodium hydrogencarbonate; trifluoroacetic acid; more than 3 stages;

upstream raw materials:

4-methyl-1H-imidazole

3,4 difluorobenzaldehyde

Downstream raw materials:

(Z)-(S)-2-[1-[3-fluoro-4-(4-methyl-1H-imidazol-1-yl)phenyl]methylidene]-4-[(1R,2R)-2-hydroxy-1-(3,4,5-trifluorophenyl)propyl]-6-methylmorpholin-3-one

3-fluoro-4-(4-methyl-1H-imidazol-1-yl)benzoic acid

1-(4-ethynyl-2-fluorophenyl)-4-methyl-1H-imidazole

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