1-hydroxylactone

Base Information

• Chemical Name: 1-hydroxylactone
• CAS No.: 33448-80-5
• Molecular Formula: C₈H₁₂O₂
• Molecular Weight: 140.182

Synonyms:

Chemical Property of 1-hydroxylactone

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-hydroxylactone

There total 2 articles about 1-hydroxylactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

C8H14O3 (1290613-79-4) → 1-oxaspiro[4.4]nonane-2,6-dione (6053-54-9) + 1-oxaspiro[4.4]nonan-2-one (33448-80-5) + C8H12O3 (1290613-77-2)

Guidance literature:

With C₂₄H₃₂FeN₆⁽⁴⁺⁾*2F₆Sb^(1-); dihydrogen peroxide;

DOI:10.1038/nchem.967

Reference yield: 61.0%

3-cyclopentylpropionic acid (140-77-2) → 1-oxaspiro[4.4]nonane-2,6-dione (6053-54-9) + 1-oxaspiro[4.4]nonan-2-one (33448-80-5) + C8H12O3 (1290613-77-2)

Guidance literature:

With dihydrogen peroxide; methyltrifluoromethyldioxirane;

DOI:10.1038/nchem.967

Reference yield: 84.0%

1-oxaspiro[4.4]nonan-2-one (33448-80-5) + pentamethylenebis(magnesium bromide) (23708-48-7) → 1-[2-(1-Hydroxycyclopentyl)ethyl]cyclohexanol (73089-99-3)

Guidance literature:

In tetrahydrofuran;

DOI:10.1021/jo01298a016

upstream raw materials:

C₈H₁₄O₃

3-cyclopentylpropionic acid

Downstream raw materials:

1-[2-(1-Hydroxycyclopentyl)ethyl]cyclohexanol

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