Tricyclo[8.2.2.24,7]hexadeca-4,6,10,12,13,15-hexaene-5,6,11,12-t

Base Information

• Chemical Name: Tricyclo[8.2.2.24,7]hexadeca-4,6,10,12,13,15-hexaene-5,6,11,12-t
• CAS No.: 37437-90-4
• Molecular Formula: C₂₄H₂₄O₈
• Molecular Weight: 440.45
• Mol file: 37437-90-4.mol

Synonyms:Tricyclo[8.2.2.24,7]hexadeca-4,6,10,12,13,15-hexaene-5,6,11,12-t;Tricyclo[8.2.2.24,7]hexadeca-4,6,10,12,13,15-hexaene-5,6,11,12-tetracarboxylic acid, tetraMethyl ester, stereoisoMer;

Chemical Property of Tricyclo[8.2.2.24,7]hexadeca-4,6,10,12,13,15-hexaene-5,6,11,12-t

Chemical Property:

• PSA: 105.20000
• LogP: 2.71680

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Tricyclo[8.2.2.24,7]hexadeca-4,6,10,12,13,15-hexaene-5,6,11,12-t

There total 4 articles about Tricyclo[8.2.2.24,7]hexadeca-4,6,10,12,13,15-hexaene-5,6,11,12-t which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

1,2,4,5-hexatetraene (29776-96-3) + dimethyl acetylenedicarboxylate → tricyclo[8.2.2.24,7]hexadeca-4,6,10,12,13,15-hexaene-5,6,11,12-tetracarboxylic acid tetramethyl ester (37437-90-4,73209-25-3,73803-20-0)

Guidance literature:

In diethyl ether; benzene; at 45 - 70 ℃; Solvent;

DOI:10.15227/orgsyn.060.0041

Reference yield:

1,2,4,5-hexatetraene (29776-96-3) + dimethyl acetylenedicarboxylate (762-42-5) → tricyclo[8.2.2.24,7]hexadeca-4,6,10,12,13,15-hexaene-5,6,11,12-tetracarboxylic acid tetramethyl ester (37437-90-4,73209-25-3,73803-20-0)

Guidance literature:

In benzene;

Reference yield:

Di-tert-butyl acetylenedicarboxylate (66086-33-7) + 1,2,4,5-hexatetraene (29776-96-3) + dimethyl acetylenedicarboxylate (762-42-5) → <2.2>Paracyclophan-4,5,12,13-tetracarbonsaeure-tetra-tert-butylester (66086-24-6,73209-28-6,73803-19-7) + tricyclo[8.2.2.24,7]hexadeca-4,6,10,12,13,15-hexaene-5,6,11,12-tetracarboxylic acid tetramethyl ester (37437-90-4,73209-25-3,73803-20-0) + <2.2>Paracyclophan-4,5,12,13-tetracarbonsaeure-4,5-di-tert-butylester-12,13-dimethylester (73764-71-3)

Guidance literature:

In benzene; for 12h; Heating;

upstream raw materials:

1,2,4,5-hexatetraene

dimethyl acetylenedicarboxylate

Di-tert-butyl acetylenedicarboxylate

Downstream raw materials:

4,5,7,12,13-pentamethyl<2.2>paracyclophane

4,5,7,8,12,13,15-heptamethyl<2.2>paracyclophane

5,6,11,13,14,16-Hexamethyl-tricyclo[8.2.2.2^4,7]hexadeca-1⁽¹³⁾,4⁽¹⁶⁾,5,7⁽¹⁵⁾,10⁽¹⁴⁾,11-hexaene

4,5,15,16-tetramethyl<2.2>paracyclophane

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