3-hydrazinyl-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Base Information

Chemical Name:3-hydrazinyl-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine
CAS No.:802598-74-9
Molecular Formula:C13H14N4
Molecular Weight:226.28
Hs Code.:
Mol file:802598-74-9.mol

Synonyms:6,7-Dichloroindole-3-acetic acid;1H-Indole-3-acetic acid,6,7-dichloro;6,7-Dichlor-3-indolylessigsaeure;6,7-dichloroindol-3-yl acetic acid;

Suppliers and Price of 3-hydrazinyl-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Chemenu
3-Hydrazino-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine 95%+
1g
$ 1577.00

Chemenu
3-Hydrazino-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine 95%+
250mg
$ 478.00

Chemenu
3-Hydrazino-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine 95%+
100mg
$ 299.00

AccelPharmtech
3-hydrazinyl-6,7-dihydro-5H-Benzo[6,7]cyclohepta[1,2-c]pyridazine 97.00%
25G
$ 10900.00

Total 6 raw suppliers

Chemical Property of 3-hydrazinyl-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Chemical Property:

Boiling Point:432.6±38.0 °C(Predicted)
PKA:6.01±0.20(Predicted)
PSA：67.06000
Density:1.35±0.1 g/cm3(Predicted)
LogP:2.04010
Storage Temp.:Keep in dark place,Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:

97% ^*data from raw suppliers

3-Hydrazino-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine 95%+ ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-hydrazinyl-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

There total 8 articles about 3-hydrazinyl-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 25823-53-4
3-chloro-2,5,6,7-tetrahydro-3H-benzo[6,7]cyclohepta[1,2-c]pyridazine

: 802598-74-9
3-hydrazino-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Guidance literature:: With hydrazine; In ethanol; at 100 ℃; for 4.75 - 16h; Product distribution / selectivity; Heating / reflux;

Reference yield:

: 826-73-3
1-Benzosuberone

: 802598-74-9
3-hydrazino-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / ethanol; water monomer / 1 h / 20 °C / Reflux

1.2: 1 h / 100 °C

1.3: 3 h / Reflux

2.1: copper chloride (II) / acetonitrile / 2 h / Reflux

3.1: trichlorophosphate / 2 h / Reflux

4.1: hydrazine / diethyl ether / 16 h / Reflux

With sodium hydroxide; copper chloride (II); hydrazine; trichlorophosphate; In diethyl ether; ethanol; water monomer; acetonitrile;

Reference yield:

: 25742-87-4
2,4,4a,5,6,7-hexahydro-3H-benzo<6,7>cyclohepta<1,2-c>pyridazin-3-one

: 802598-74-9
3-hydrazino-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Guidance literature:: Multi-step reaction with 3 steps

1: copper chloride (II) / acetonitrile / 2 h / Reflux

2: trichlorophosphate / 2 h / Reflux

3: hydrazine / diethyl ether / 16 h / Reflux

With copper chloride (II); hydrazine; trichlorophosphate; In diethyl ether; acetonitrile;