3-Chloro-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Base Information

Chemical Name:3-Chloro-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine
CAS No.:25823-53-4
Molecular Formula:C13H11 Cl N2
Molecular Weight:230.69
Hs Code.:2933990090
European Community (EC) Number:829-886-4
DSSTox Substance ID:DTXSID60556295
Wikidata:Q82437805
Mol file:25823-53-4.mol

Synonyms:25823-53-4;3-Chloro-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine;5-chloro-3,4-diazatricyclo[9.4.0.02,7]pentadeca-1(15),2,4,6,11,13-hexaene;5H-Benzo[6,7]cyclohepta[1,2-c]pyridazine, 3-chloro-6,7-dihydro-;5H-Benzo[6,7]cyclohepta[1,2-c]pyridazine,3-chloro-6,7-dihydro-;SCHEMBL467676;DTXSID60556295;PJMKITDIWYPIHU-UHFFFAOYSA-N;MFCD06801335;AKOS012080790;EN300-251568;G62896;Z1013743640;5-chloro-3, 4-diazatricyclo[9.4.0.02, 7]pentadeca-1(15), 2, 4, 6, 11, 13-hexaene;5-chloro-3,4-diazatricyclo[9.4.0.0,2,7]pentadeca-1(15),2(7),3,5,11,13-hexaene

Suppliers and Price of 3-Chloro-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Chloro-3,4-diazatricyclo[9.4.0.0,2,7]pentadeca-1(15),2(7),3,5,11,13-hexaene
50mg
$ 220.00

TRC
5-Chloro-3,4-diazatricyclo[9.4.0.0,2,7]pentadeca-1(15),2(7),3,5,11,13-hexaene
10mg
$ 65.00

SynQuest Laboratories
3-Chloro-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine
250 mg
$ 816.00

American Custom Chemicals Corporation
3-CHLORO-6,7-DIHYDRO-5H-BENZO[6,7]CYCLOHEPTA[1,2-C]PYRIDAZINE 95.00%
250MG
$ 938.42

American Custom Chemicals Corporation
3-CHLORO-6,7-DIHYDRO-5H-BENZO[6,7]CYCLOHEPTA[1,2-C]PYRIDAZINE 95.00%
100MG
$ 787.06

AK Scientific
3-Chloro-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine
250mg
$ 648.00

Total 10 raw suppliers

Chemical Property of 3-Chloro-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Chemical Property:

Melting Point:159 °C(Solv: methanol (67-56-1))
Boiling Point:465.4°Cat760mmHg
PKA:1.24±0.20(Predicted)
Flash Point:267.7°C
PSA：25.78000
Density:1.266g/cm³
LogP:3.28570
XLogP3:3.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:230.0610761
Heavy Atom Count:16
Complexity:246

Purity/Quality:

99% ,99.9%, ^*data from raw suppliers

5-Chloro-3,4-diazatricyclo[9.4.0.0,2,7]pentadeca-1(15),2(7),3,5,11,13-hexaene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=CC=CC=C2C3=NN=C(C=C3C1)Cl

Technology Process of 3-Chloro-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine

There total 7 articles about 3-Chloro-6,7-dihydro-5H-benzo[6,7]cyclohepta[1,2-c]pyridazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 25823-52-3
2,5,6,7-tetrahydro-3H-benzo[6,7]cyclohepta[1,2-c]pyridazin-3-one

: 25823-53-4
3-chloro-2,5,6,7-tetrahydro-3H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Guidance literature:: 2,5,6,7-tetrahydro-3H-benzo[6,7]cyclohepta[1,2-c]pyridazin-3-one; With trichlorophosphate; at 100 ℃; for 2 - 4.75h; Heating / reflux;

With water; sodium hydrogencarbonate; at 0 ℃; Product distribution / selectivity;

Reference yield:

: 826-73-3
1-Benzosuberone

: 25823-53-4
3-chloro-2,5,6,7-tetrahydro-3H-benzo[6,7]cyclohepta[1,2-c]pyridazine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / ethanol; water monomer / 1 h / 20 °C / Reflux

1.2: 1 h / 100 °C

1.3: 3 h / Reflux

2.1: copper chloride (II) / acetonitrile / 2 h / Reflux

3.1: trichlorophosphate / 2 h / Reflux

With sodium hydroxide; copper chloride (II); trichlorophosphate; In ethanol; water monomer; acetonitrile;