TERT-BUTYL METHYL 1H-INDAZOLE-1,6-DICARBOXYLATE

Base Information

• Chemical Name: TERT-BUTYL METHYL 1H-INDAZOLE-1,6-DICARBOXYLATE
• CAS No.: 1126424-50-7
• Molecular Formula: C14H16N2O4
• Molecular Weight: 276.29
• Hs Code.: 2933990090
• Mol file: 1126424-50-7.mol

Synonyms:1-O-tert-butyl 6-O-methyl indazole-1,6-dicarboxylate;

Chemical Property of TERT-BUTYL METHYL 1H-INDAZOLE-1,6-DICARBOXYLATE

Chemical Property:

• PSA: 70.42000
• LogP: 2.60610
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

1-tert-Butyl6-Methyl1H-Indazole-1,6-dicarboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TERT-BUTYL METHYL 1H-INDAZOLE-1,6-DICARBOXYLATE

There total 1 articles about TERT-BUTYL METHYL 1H-INDAZOLE-1,6-DICARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

di-tert-butyl dicarbonate (24424-99-5) + 1H-indazole-6-carboxylic acid methyl ester (170487-40-8) → 1-tert-butyl 6-methyl 1H-indazole-1,6-dicarboxylate (1126424-50-7)

Guidance literature:

With dmap; triethylamine; In tetrahydrofuran; at 20 ℃; Cooling with ice;

Reference yield: 40.0%

1-tert-butyl 6-methyl 1H-indazole-1,6-dicarboxylate (1126424-50-7) → tert-butyl 6-(hydroxymethyl)-1H-indazole-1-carboxylate (1126424-52-9) + 1H-indazole-6-carboxylic acid methyl ester (170487-40-8)

Guidance literature:

1-tert-butyl 6-methyl 1H-indazole-1,6-dicarboxylate; With lithium triethylborohydride; In tetrahydrofuran; at -78 ℃; for 1h;

With sodium hydrogen sulfate; water; In tetrahydrofuran; Product distribution / selectivity;

Reference yield: 14.0%

1-tert-butyl 6-methyl 1H-indazole-1,6-dicarboxylate (1126424-50-7) → tert-butyl 6-(hydroxymethyl)-1H-indazole-1-carboxylate (1126424-52-9)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at -30 ℃; for 1.5h;

upstream raw materials:

di-tert-butyl dicarbonate

1H-indazole-6-carboxylic acid methyl ester

Downstream raw materials:

tert-butyl 6-(hydroxymethyl)-1H-indazole-1-carboxylate

1H-indazole-6-carboxylic acid methyl ester

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