4,4,5,5-tetraMethyl-2-(3-(triphenylen-2-yl)phenyl)-1,3,2-dioxaborolane

Base Information

• Chemical Name: 4,4,5,5-tetraMethyl-2-(3-(triphenylen-2-yl)phenyl)-1,3,2-dioxaborolane
• CAS No.: 1115639-92-3
• Molecular Formula: C30H27BO2
• Molecular Weight: 430.354
• Hs Code.: 2931900090
• Mol file: 1115639-92-3.mol

Synonyms:4,4,5,5-tetramethyl-2-(3-(triphenylen-2-yl)phenyl)-1,3,2-dioxaborolane

Chemical Property of 4,4,5,5-tetraMethyl-2-(3-(triphenylen-2-yl)phenyl)-1,3,2-dioxaborolane

Chemical Property:

• Melting Point: 177.0 to 181.0 °C
• Boiling Point: 630.5±34.0 °C(Predicted)
• PSA: 18.46000
• Density: 1.18±0.1 g/cm3(Predicted)
• LogP: 7.11240
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

98% ^*data from raw suppliers

4,4,5,5-Tetramethyl-2-[3-(triphenylen-2-yl)phenyl]-1,3,2-dioxaborolane >98.0%(GC)(T) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4,4,5,5-tetraMethyl-2-(3-(triphenylen-2-yl)phenyl)-1,3,2-dioxaborolane

There total 6 articles about 4,4,5,5-tetraMethyl-2-(3-(triphenylen-2-yl)phenyl)-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.2%

2-(3-chlorophenyl)triphenylene + bis(pinacol)diborane (73183-34-3) → 4,4,5,5-tetramethyl-2-(3-(triphenylene-2-yl) phenyl)-1,3,2-dioxaborolane (1115639-92-3)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In N,N-dimethyl-formamide; at 150 ℃; for 12h;

Reference yield: 72.0%

→ 4,4,5,5-tetramethyl-2-(3-(triphenylene-2-yl) phenyl)-1,3,2-dioxaborolane (1115639-92-3)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 95 ℃; for 24h;

Reference yield: 71.0%

2-(3-bromophenyl)triphenylene (1313514-53-2) + bis(pinacol)diborane (73183-34-3) → 4,4,5,5-tetramethyl-2-(3-(triphenylene-2-yl) phenyl)-1,3,2-dioxaborolane (1115639-92-3)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 95 ℃; for 24h;

upstream raw materials:

2-bromobenzo[9,10]phenanthrene

3-chlorophenylboronic acid

bis(pinacol)diborane

2-(3-bromophenyl)triphenylene

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