1-(2-Hydroxyphenyl)-3-(3-methylphenyl)propane-1,3-dione

Base Information

Chemical Name:1-(2-Hydroxyphenyl)-3-(3-methylphenyl)propane-1,3-dione
CAS No.:420823-93-4
Molecular Formula:C16H14O3
Molecular Weight:254.285
Hs Code.:
DSSTox Substance ID:DTXSID20357982
Wikidata:Q82138207
Mol file:420823-93-4.mol

Synonyms:420823-93-4;1-(2-hydroxyphenyl)-3-(3-methylphenyl)propane-1,3-dione;1-(2-Hydroxyphenyl)-3-(m-tolyl)propane-1,3-dione;Oprea1_695924;DTXSID20357982;MFCD20502992;AKOS022184463;BS-37777;SR-01000221093;SR-01000221093-1

Suppliers and Price of 1-(2-Hydroxyphenyl)-3-(3-methylphenyl)propane-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1-(2-Hydroxyphenyl)-3-(3-methylphenyl)propane-1,3-dione

Chemical Property:

Vapor Pressure:2.6E-08mmHg at 25°C
Boiling Point:438.8°C at 760 mmHg
Flash Point:233.3°C
Density:1.201g/cm³
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:254.094294304
Heavy Atom Count:19
Complexity:337

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)C(=O)CC(=O)C2=CC=CC=C2O

Technology Process of 1-(2-Hydroxyphenyl)-3-(3-methylphenyl)propane-1,3-dione

There total 4 articles about 1-(2-Hydroxyphenyl)-3-(3-methylphenyl)propane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2-(dimethyl(oxo)- λ⁶-sulfanylidene)-1-(m-tolyl)ethan-1-one

: 90-02-8
salicylaldehyde

: 420823-93-4
1-(2-hydroxyphenyl)-3-(m-tolyl)propane-1,3-dione

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; sodium acetate; In 1,2-dichloro-ethane; at 90 ℃; for 24h;
DOI:10.1002/adsc.201900276

Reference yield:

: 1711-06-4
3-Methylbenzoyl chloride

: 420823-93-4
1-(2-hydroxyphenyl)-3-(m-tolyl)propane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: benzene

With pyridine; benzene;

Reference yield:

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 420823-93-4
1-(2-hydroxyphenyl)-3-(m-tolyl)propane-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 0.2 h / 20 °C

2: sodium hydroxide / pyridine / 2 h / 70 °C

With pyridine; sodium hydroxide; In pyridine;
DOI:10.1002/chem.201901781