8-BROMO-1,3,4,5-TETRAHYDRO-2H-1,5-BENZODIAZEPIN-2-ONE

Base Information

Chemical Name:8-BROMO-1,3,4,5-TETRAHYDRO-2H-1,5-BENZODIAZEPIN-2-ONE
CAS No.:37040-46-3
Molecular Formula:C₉H₉BrN₂O
Molecular Weight:241.087
Hs Code.:
Mol file:37040-46-3.mol

Synonyms:8-BROMO-1,3,4,5-TETRAHYDRO-2H-1,5-BENZODIAZEPIN-2-ONE;8-bromo-4,5-dihydro-1H-benzo[b][1,4]diazepin-2(3H)-one

Suppliers and Price of 8-BROMO-1,3,4,5-TETRAHYDRO-2H-1,5-BENZODIAZEPIN-2-ONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
8-Bromo-4,5-dihydro-1H-benzo[b][1,4]diazepin-2(3H)-one 95+%
5g
$ 1632.00

Crysdot
8-Bromo-4,5-dihydro-1H-benzo[b][1,4]diazepin-2(3H)-one 95+%
1g
$ 465.00

Chemenu
8-Bromo-4,5-dihydro-1H-benzo[b][1,4]diazepin-2(3H)-one 95%
1g
$ 439.00

Alichem
8-Bromo-4,5-dihydro-1h-benzo[b][1,4]diazepin-2(3h)-one
5g
$ 1749.32

Total 3 raw suppliers

Chemical Property of 8-BROMO-1,3,4,5-TETRAHYDRO-2H-1,5-BENZODIAZEPIN-2-ONE

Chemical Property:

PSA：41.13000
LogP:2.47920

Purity/Quality:

99% ^*data from raw suppliers

8-Bromo-4,5-dihydro-1H-benzo[b][1,4]diazepin-2(3H)-one 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 8-Bromo-1,3,4,5-Tetrahydro-2h-1,5-Benzodiazepin-2-One is used in preparation of bromobenzodiazepinones by direct electrophilic bromination of tetrahydrobenzodiazepinones.

Technology Process of 8-BROMO-1,3,4,5-TETRAHYDRO-2H-1,5-BENZODIAZEPIN-2-ONE

There total 5 articles about 8-BROMO-1,3,4,5-TETRAHYDRO-2H-1,5-BENZODIAZEPIN-2-ONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 5755-07-7
2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-2-one

: 37040-46-3
8-bromo-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one

: 6,8-dibromo-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one

Guidance literature:: With bromine; In chloroform; at 5 ℃; for 4h;
DOI:10.1007/BF02297679

Reference yield:

: C₉H₁₁BrN₂O₂

: 37040-46-3
8-bromo-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one

Guidance literature:: With sulfuric acid; In acetonitrile; at 80 ℃; for 1h;

Reference yield:

: 1250649-95-6
C₁₀H₁₃BrN₂O₂

: 37040-46-3
8-bromo-1,3,4,5-tetrahydro-benzo[b][1,4]diazepin-2-one

Guidance literature:: C₁₀H₁₃BrN₂O₂; With sulfuric acid; In acetonitrile; at 80 ℃; for 1h;

With sodium hydrogencarbonate; In dichloromethane; water; acetonitrile;