DPA-DC1

Base Information

Chemical Name:DPA-DC1
CAS No.:819066-98-3
Molecular Formula:C36H41N7O
Molecular Weight:587.768
Hs Code.:
Mol file:819066-98-3.mol

Synonyms:DPA-DC1;5-(4-Aminobutoxy)-N,N,N',N'-tetrakis(2-pyridinylmethyl)-1,3-benzenedimethanamine

Suppliers and Price of DPA-DC1

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N,N'-((5-(4-Aminobutoxy)-1,3-phenylene)bis(methylene))bis(1-(pyridin-2-yl)-N-(pyridin-2-ylmethyl)methanamine) 97%
1g
$ 990.00

Alichem
N,N'-((5-(4-Aminobutoxy)-1,3-phenylene)bis(methylene))bis(1-(pyridin-2-yl)-N-(pyridin-2-ylmethyl)methanamine)
1g
$ 824.00

Total 5 raw suppliers

Chemical Property of DPA-DC1

Chemical Property:

PSA：93.29000
LogP:6.48940

Purity/Quality:

98% ^*data from raw suppliers

N,N'-((5-(4-Aminobutoxy)-1,3-phenylene)bis(methylene))bis(1-(pyridin-2-yl)-N-(pyridin-2-ylmethyl)methanamine) 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of DPA-DC1

There total 10 articles about DPA-DC1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 819066-97-2
2-(4-{3,5-bis-[(bis-pyridin-2-ylmethyl-amino)-methyl]-phenoxy}-butyl)-isoindole-1,3-dione

: 819066-98-3
N,N'-(5-(4-aminobutoxy)-1,3-phenylene)bis(methylene)bis(1-(pyridin-2-yl)-N-(pyridin-2-ylmethyl)methanamine)

Guidance literature:: With hydrazine; In ethanol; at 20 ℃; for 18h; Reflux;

Reference yield:

: C₄₁H₄₉N₇O₃

: 819066-98-3
N,N'-(5-(4-aminobutoxy)-1,3-phenylene)bis(methylene)bis(1-(pyridin-2-yl)-N-(pyridin-2-ylmethyl)methanamine)

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; Cooling with ice;

Reference yield:

: 618-83-7
5-Hydroxyisophthalic acid

: 819066-98-3
N,N'-(5-(4-aminobutoxy)-1,3-phenylene)bis(methylene)bis(1-(pyridin-2-yl)-N-(pyridin-2-ylmethyl)methanamine)

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / H₂SO₄ / Heating

2: 96 percent / LiAlH₄ / tetrahydrofuran / 0 - 20 °C

3: 90 percent / K₂CO₃ / acetonitrile / 24 h / Heating

4: 89 percent / CBr₄; Ph₃P / CH₂Cl₂ / 20 °C

5: 91 percent / K₂CO₃ / dimethylformamide

6: hydrazine hydrate / CH₂Cl₂; ethanol / 1 h / Heating

With lithium aluminium tetrahydride; carbon tetrabromide; sulfuric acid; potassium carbonate; hydrazine hydrate; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2004.08.052