1H-IMidazole, 4-broMo-1-Methyl-2-phenyl-

Base Information

Chemical Name:1H-IMidazole, 4-broMo-1-Methyl-2-phenyl-
CAS No.:86119-59-7
Molecular Formula:C10H9BrN2
Molecular Weight:237.09586
Hs Code.:2933299090
Mol file:86119-59-7.mol

Synonyms:1H-IMidazole, 4-broMo-1-Methyl-2-phenyl-

Suppliers and Price of 1H-IMidazole, 4-broMo-1-Methyl-2-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynQuest Laboratories
4-Bromo-1-methyl-2-phenyl-1H-imidazole 98.0%
5 g
$ 1548.00

Chemenu
4-Bromo-1-methyl-2-phenyl-1H-imidazole 95%+
5g
$ 1394.00

Chemenu
4-Bromo-1-methyl-2-phenyl-1H-imidazole 95%+
1g
$ 403.00

Chemenu
4-Bromo-1-methyl-2-phenyl-1H-imidazole 95%+
250mg
$ 233.00

Chemenu
4-Bromo-1-methyl-2-phenyl-1H-imidazole 95%+
100mg
$ 121.00

Total 9 raw suppliers

Chemical Property of 1H-IMidazole, 4-broMo-1-Methyl-2-phenyl-

Chemical Property:

Melting Point:66-68 °C
Boiling Point:360.3±34.0 °C(Predicted)
PKA:3.85±0.60(Predicted)
PSA：17.82000
Density:1.44±0.1 g/cm3(Predicted)
LogP:2.84960

Purity/Quality:

NLT 98% ^*data from raw suppliers

4-Bromo-1-methyl-2-phenyl-1H-imidazole 98.0% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 4-Bromo-1-methyl-2-phenyl-1H-imidazole is used in the preparation of new ligands bearing imidazole groups.

Technology Process of 1H-IMidazole, 4-broMo-1-Methyl-2-phenyl-

There total 2 articles about 1H-IMidazole, 4-broMo-1-Methyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 86119-58-6
2-phenyl-4⁽⁵⁾-bromoimidazole

: 74-88-4
methyl iodide

: 86119-59-7
4-bromo-1-methyl-2-phenyl-1H-imidazole

: 71045-44-8
5-bromo-1-methyl-2-phenyl-1H-imidazole

Guidance literature:: With sodium hydride; In tetrahydrofuran; 1.) 0 deg C -> RT, 30 min, 2.) 0 deg C -> RT, 12 h;
DOI:10.1021/ja00354a025

Reference yield:

: 56338-00-2
4,5-dibromo-2-phenyl-1H-imidazole

: 86119-59-7
4-bromo-1-methyl-2-phenyl-1H-imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: 51 percent / Na₂SO₃ / aq. ethanol / 46 h / Heating

2: 57 percent / NaH / tetrahydrofuran / 1.) 0 deg C -> RT, 30 min, 2.) 0 deg C -> RT, 12 h

With sodium hydride; sodium sulfite; In tetrahydrofuran; ethanol;
DOI:10.1021/ja00354a025

Reference yield: 38.0%

: 86119-59-7
4-bromo-1-methyl-2-phenyl-1H-imidazole

: 105-58-8,76619-83-5
Diethyl carbonate

: 86119-60-0
N-methyl-2-phenyl-4-carbethoxyimidazole

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 30 min, 2.) -78 deg C -> -40 deg C, 30 min;
DOI:10.1021/ja00354a025