Technology Process of 2-(4-AMINOPHENOXYMETHYL)-2,5,7,8-TETRAMETHYL-4-OXOCHROMAN-6-YL ACETATE
There total 6 articles about 2-(4-AMINOPHENOXYMETHYL)-2,5,7,8-TETRAMETHYL-4-OXOCHROMAN-6-YL ACETATE which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol; benzene;
for 3h;
under 2325.2 - 2850.2 Torr;
DOI:10.1021/jm00122a022
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) NaH / 1.) DMF, rt, 1 h, 2.) benzene, rt, 1 h
2: 1.) NaH / 1.) DMSO, benzene, 60 deg C, 20 min, 2.) 60 deg C, 1 h
3: 94 percent / AcOH, 10percent H2SO4 / 0.17 h / 60 °C
4: 94 percent / pyridine / 1.) 10 deg C to rt, 2.) 30 deg C, 1 h
5: 98 percent / H2 / 10percent Pd-C / methanol; benzene / 3 h / 2325.2 - 2850.2 Torr
With
pyridine; sulfuric acid; hydrogen; sodium hydride; acetic acid;
palladium on activated charcoal;
In
methanol; benzene;
DOI:10.1021/jm00122a022
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) NaH / 1.) DMSO, benzene, 60 deg C, 20 min, 2.) 60 deg C, 1 h
2: 94 percent / AcOH, 10percent H2SO4 / 0.17 h / 60 °C
3: 94 percent / pyridine / 1.) 10 deg C to rt, 2.) 30 deg C, 1 h
4: 98 percent / H2 / 10percent Pd-C / methanol; benzene / 3 h / 2325.2 - 2850.2 Torr
With
pyridine; sulfuric acid; hydrogen; sodium hydride; acetic acid;
palladium on activated charcoal;
In
methanol; benzene;
DOI:10.1021/jm00122a022