tert-Butyl (3-(4-cyanophenyl)oxetan-3-yl)carbamate

Base Information

• Chemical Name: tert-Butyl (3-(4-cyanophenyl)oxetan-3-yl)carbamate
• CAS No.: 1158098-77-1
• Molecular Formula: C15H18N2O3
• Molecular Weight: 274.32
• Hs Code.: 2932999099
• Mol file: 1158098-77-1.mol

Synonyms:tert-Butyl (3-(4-cyanophenyl)oxetan-3-yl)carbamate;3-Boc-aMino-3-(4-cyanophenyl)oxetane;tert-butyl N-[3-(4-cyanophenyl)oxetan-3-yl]carbamate

Chemical Property of tert-Butyl (3-(4-cyanophenyl)oxetan-3-yl)carbamate

Chemical Property:

• PSA: 74.84000
• LogP: 2.51288

Purity/Quality:

99%, ^*data from raw suppliers

3-Boc-Amino-3-(4-cyanophenyl)oxetane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-Butyl (3-(4-cyanophenyl)oxetan-3-yl)carbamate

There total 1 articles about tert-Butyl (3-(4-cyanophenyl)oxetan-3-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + 2-methyl-propane-2-sulfinic acid [3-(4-cyano-phenyl)-oxetan-3-yl]-amide (1158098-76-0) → [3-(4-cyano-phenyl)-oxetan-3-yl]-carbamic acid tert-butyl ester (1158098-77-1)

Guidance literature:

2-methyl-propane-2-sulfinic acid [3-(4-cyano-phenyl)-oxetan-3-yl]-amide; With hydrogenchloride; In diethyl ether; dichloromethane; cyclohexane; at 20 ℃; for 0.666667h;

di-tert-butyl dicarbonate; With sodium hydroxide; dmap; In 1,4-dioxane; water; at 20 ℃; for 16h;

Reference yield:

[3-(4-cyano-phenyl)-oxetan-3-yl]-carbamic acid tert-butyl ester (1158098-77-1) → {3-[4-(N-hydroxycarbamimidoyl)-phenyl]-oxetan-3-yl}-carbamic acid tert-butyl ester (1158098-79-3)

Guidance literature:

With hydroxylamine; In tetrahydrofuran; water; at 20 ℃; for 48h;

upstream raw materials:

di-tert-butyl dicarbonate

2-methyl-propane-2-sulfinic acid [3-(4-cyano-phenyl)-oxetan-3-yl]-amide

Downstream raw materials:

{3-[4-(N-hydroxycarbamimidoyl)-phenyl]-oxetan-3-yl}-carbamic acid tert-butyl ester

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