1H-Pyrazole-3,5-dicarboxaMide

Base Information

• Chemical Name: 1H-Pyrazole-3,5-dicarboxaMide
• CAS No.: 1397683-79-2
• Molecular Formula: C5H6N4O2
• Molecular Weight: 154.12674
• Hs Code.: 2933199090
• Mol file: 1397683-79-2.mol

Synonyms:1H-Pyrazole-3,5-dicarboxaMide;1H-Pyrazole-3,5-dicarboxylic acid diamide

Chemical Property of 1H-Pyrazole-3,5-dicarboxaMide

Chemical Property:

• PSA: 115.85000
• LogP: 0.19200
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

1H-Pyrazole-3,5-dicarboxamide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Pyrazole-3,5-dicarboxaMide

There total 3 articles about 1H-Pyrazole-3,5-dicarboxaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

diethyl 1H-pyrazole-3,5-dicarboxylate (37687-24-4) → 1H-pyrazole-3,5-dicarboxamide (1397683-79-2)

Guidance literature:

With ammonia; In methanol; at 70 ℃; for 48h; Sealed tube;

Reference yield: 95.0%

3,5-(1H)-pyrazoledicarbaldehyde (148832-75-1) → 1H-pyrazole-3,5-dicarboxamide (1397683-79-2)

Guidance literature:

With hydroxylamine; C₃₃H₂₈F₃N₅O₃Ru⁽¹⁺⁾*Cl^(1-); In water; at 60 ℃; Sonication;

DOI:10.1246/BCSJ.20200071

Reference yield: 52.6%

3,5-dicarbomethoxypyrazole (4077-76-3) → 1H-pyrazole-3,5-dicarboxamide (1397683-79-2)

Guidance literature:

With ammonia; In methanol; at 70 ℃; for 48h; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1021/jacs.7b08629

upstream raw materials:

diethyl 1H-pyrazole-3,5-dicarboxylate

3,5-dicarbomethoxypyrazole

3,5-(1H)-pyrazoledicarbaldehyde

Downstream raw materials:

1H-pyrazole-3,5-dicarbonitrile

bis(3,5-aminomethyl)pyrazole

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