Bis[1,3-bis(diphenylphosphino)propane]rhodium Tetrafluoroborate

Base Information

Chemical Name:Bis[1,3-bis(diphenylphosphino)propane]rhodium Tetrafluoroborate
CAS No.:70196-21-3
Molecular Formula:BF₄*C₅₄H₅₂P₄Rh
Molecular Weight:0
Hs Code.:

Synonyms:Bis[1,3-bis(diphenylphosphino)propane]rhodium Tetrafluoroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Bis[1,3-bis(diphenylphosphino)propane]rhodium Tetrafluoroborate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Bis[1,3-bis(diphenylphosphino)propane]rhodium Tetrafluoroborate

There total 4 articles about Bis[1,3-bis(diphenylphosphino)propane]rhodium Tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65606-90-8
Rh⁽¹⁺⁾*((C₆H₅)2PCH₂CH₂CH₂P(C₆H₅)2)*C₇H₈*BF₄^(1-)={Rh((C₆H₅)2PCH₂CH₂CH₂P(C₆H₅)2)(C₇H₈)}BF₄

: 6737-42-4
1,3-bis-(diphenylphosphino)propane

: 70196-21-3
Rhodiumbis(1,3-bis(diphenylphosphino)propane) tetrafluoroborate

Guidance literature:: In methanol; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.jorganchem.2019.02.009

Reference yield:

: acethylacetonato(1,5-cyclooctadiene)rhodium(I)

: 6737-42-4
1,3-bis-(diphenylphosphino)propane

: 70196-21-3
[Rh(1,3-bis(diphenylphosphino)propane)2]BF₄

Guidance literature:: With trityl tetrafluoroborate; In dichloromethane; to a soln. of Rh complex in CH2CH2, a soln. of the appropriate amt. of Ph2P(CH2)3PPh2 is added at 0°C; soln. concd. in vac., addn. of Et2O, compd. sepd.; recrystd. from dichloromethane/ether;
DOI:10.1016/0022-328X(85)87071-6

Reference yield:

: [(C,N-1-(6-mesityl-2-picolyl)-3-mesitylimidazol-2-ylidene)Rh(1,5-cyclooctadiene)]BF₄

: 6737-42-4
1,3-bis-(diphenylphosphino)propane

: (1,3-bis(diphenylphosphino)propane)2Rh(O)2BF₄

: 70196-21-3
[Rh(1,3-bis(diphenylphosphino)propane)2]BF₄

Guidance literature:: With air; In chloroform-d1; Sonication; P ligand and Rh complex were dissolved in CDCl3 under N2 with sonication; mixt. was exposed to air for 24 h; NMR monitoring;
DOI:10.1016/j.jorganchem.2006.06.004