Methanesulfonic acid 4-trifluoroMethyl-cyclohexyl ester

Base Information

• Chemical Name: Methanesulfonic acid 4-trifluoroMethyl-cyclohexyl ester
• CAS No.: 1544010-54-9
• Molecular Formula: C8H13F3O3S
• Molecular Weight: 246.251
• Mol file: 1544010-54-9.mol

Synonyms:Methanesulfonic acid 4-trifluoroMethyl-cyclohexyl ester;4-(trifluoromethyl)cyclohexyl methanesulfonate

Chemical Property of Methanesulfonic acid 4-trifluoroMethyl-cyclohexyl ester

Chemical Property:

• Boiling Point: 298.9±35.0 °C(Predicted)
• PSA: 51.75000
• Density: 1.32±0.1 g/cm3(Predicted)
• LogP: 3.16450

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methanesulfonic acid 4-trifluoroMethyl-cyclohexyl ester

There total 1 articles about Methanesulfonic acid 4-trifluoroMethyl-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(trifluoromethyl)cyclohexan-1-ol (75091-92-8,75091-93-9,30129-18-1) + methanesulfonyl chloride (124-63-0) → trans-4-(trifluoromethyl)cyclohexyl methanesulfonate (1544010-47-0) + cis-4-(trifluoromethyl)cyclohexyl methanesulfonate (1544010-54-9)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; Overall yield = 82 %; Overall yield = 23.9 g;

Reference yield: 65.0%

cis-4-(trifluoromethyl)cyclohexyl methanesulfonate (1544010-54-9) + methyl 6-hydroxynaphthalene-2-carboxylate (17295-11-3) → methyl 6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate (1544664-36-9)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 16h;

upstream raw materials:

4-(trifluoromethyl)cyclohexan-1-ol

methanesulfonyl chloride

Downstream raw materials:

methyl 6-((cis-4-(trifluoromethyl)cyclohexyl)oxy)-2-naphthoate

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