sodium ethyl(phenyl)carbamodithioate

Base Information

• Chemical Name: sodium ethyl(phenyl)carbamodithioate
• CAS No.: 13074-29-8
• Molecular Formula: C9H11 N S2 . Na
• Molecular Weight: 219.307
• Mol file: 13074-29-8.mol

Synonyms:Carbamodithioicacid, ethylphenyl-, sodium salt (9CI); Carbanilic acid, N-ethyldithio-, sodiumsalt (8CI); Sodium N-ethyl-N-phenyldithiocarbamate; Sodiumethyldithiocarbanilate; Sodium ethylphenyldithiocarbamate

Chemical Property of sodium ethyl(phenyl)carbamodithioate

Chemical Property:

• Vapor Pressure: 0.00707mmHg at 25°C
• Boiling Point: 269.9°Cat760mmHg
• Flash Point: 117°C
• Density: g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sodium ethyl(phenyl)carbamodithioate

There total 1 articles about sodium ethyl(phenyl)carbamodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

carbon disulfide (75-15-0,12122-00-8) + N-ethyl-N-phenylamine (103-69-5) → (N-ethyl-N'-phenyl-dithiocarbamato) sodium (13074-29-8)

Guidance literature:

With sodium hydroxide; In methanol; water; at 0 - 4 ℃; for 7h;

DOI:10.1080/17415993.2019.1703986

Reference yield: 92.0%

dichloro(1,5-cyclooctadiene)platinum(ll) (12080-32-9) + (N-ethyl-N'-phenyl-dithiocarbamato) sodium (13074-29-8) + poly[{μ3-4-[(pyrimidin-2-ylazanidyl)sulfonyl]aniline}sodium(I)] (547-32-0) → [Pt(SD)(et-DTC)]

Guidance literature:

dichloro(1,5-cyclooctadiene)platinum(ll); poly[{μ₃-4-[(pyrimidin-2-ylazanidyl)sulfonyl]aniline}sodium(I)]; In water; for 1h; Reflux;

(N-ethyl-N'-phenyl-dithiocarbamato) sodium; In water; for 3h; Reflux;

DOI:10.4314/bcse.v27i1.8

Reference yield: 88.0%

copper(II) nitrate trihydrate + (N-ethyl-N'-phenyl-dithiocarbamato) sodium (13074-29-8) → C18H20CuN2S4

Guidance literature:

In ethanol; for 1h;

DOI:10.1007/s11164-016-2709-2

upstream raw materials:

carbon disulfide

N-ethyl-N-phenylamine

Downstream raw materials:

N,N'-diethyl-N,N'-diphenylthiuram disulfide

{Cu(SSCN(C₂H₅)(C₆H₅))2}

di-p-tert-butylphenyltin(IV)-bis-N,N-ethylphenyldithiocarbamate

Co((C₂H₅)(C₆H₅)NCS₂)3

Refernces

• 1、 Oluwalana, Abimbola E.,Ajibade, Peter A.. "Synthesis and crystal structures of Pb(II) dithiocarbamates complexes: precursors for PbS nanophotocatalyst". . p. 182 - 199. Retrieved 2020.
• 2、 Onwudiwe, Damian C.,Ekennia, Anthony C.. "Synthesis, characterization, thermal, antimicrobial and antioxidant studies of some transition metal dithiocarbamates". . p. 1465 - 1485. Retrieved 2017/02/15.