Rhuscholide A

Base Information

Chemical Name:Rhuscholide A
CAS No.:944804-58-4
Molecular Formula:C₃₁H₄₂O₃
Molecular Weight:462.673
Hs Code.:
Mol file:944804-58-4.mol

Synonyms:Rhuscholide A

Suppliers and Price of Rhuscholide A

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
RhuscholideA ≥98%
5mg
$ 643.00

Total 12 raw suppliers

Chemical Property of Rhuscholide A

Chemical Property:

PSA：46.53000
LogP:8.79280

Purity/Quality:

98%Min ^*data from raw suppliers

RhuscholideA ≥98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Rhuscholide A

There total 14 articles about Rhuscholide A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 67-64-1
acetone

: 5-hydroxy-7-(3,7,11,15-tetramethyl-2,6,10,11-hexadecatetraenyl)-2(3H)-benzofuranone

: 944804-58-4
rhuscholide A

Guidance literature:: With piperidine; In ethanol; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2019.151059

Reference yield:

: acetic acid 2-allyl-4-benzyloxyphenyl ester

: 944804-58-4
rhuscholide A

Guidance literature:: Multi-step reaction with 10 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tert-butyl alcohol; tetrahydrofuran; water / 12 h / 20 °C / Inert atmosphere

2.1: sodium periodate / water; methanol / 2 h / 0 °C / Inert atmosphere

3.1: pyridinium p-toluenesulfonate / benzene / 2 h / Reflux; Inert atmosphere

4.1: sodium hydroxide / water; methanol / 2 h / 0 °C / Inert atmosphere

5.1: sodium hydride / toluene; mineral oil / 0.5 h / 0 °C / Inert atmosphere

5.2: 12 h / 20 °C / Inert atmosphere

6.1: hydrogenchloride / tetrahydrofuran; water / 48 h / 20 °C / Inert atmosphere

7.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tert-butyl alcohol; tetrahydrofuran; water / 14 h / 20 °C / Inert atmosphere

8.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Inert atmosphere

9.1: pentamethylbenzene,; boron trichloride / dichloromethane / 0.55 h / -78 °C / Inert atmosphere

10.1: piperidine / ethanol / 3 h / 20 °C / Inert atmosphere

With piperidine; hydrogenchloride; sodium chlorite; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; 2-methyl-but-2-ene; pentamethylbenzene,; pyridinium p-toluenesulfonate; boron trichloride; sodium hydride; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; mineral oil; tert-butyl alcohol; benzene; 10.1: |Aldol Condensation;
DOI:10.1016/j.tetlet.2019.151059

Reference yield:

: C₁₉H₂₀O₅

: 944804-58-4
rhuscholide A

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydroxide / water; methanol / 2 h / 0 °C / Inert atmosphere

2.1: sodium hydride / toluene; mineral oil / 0.5 h / 0 °C / Inert atmosphere

2.2: 12 h / 20 °C / Inert atmosphere

3.1: hydrogenchloride / tetrahydrofuran; water / 48 h / 20 °C / Inert atmosphere

4.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / tert-butyl alcohol; tetrahydrofuran; water / 14 h / 20 °C / Inert atmosphere

5.1: toluene-4-sulfonic acid / toluene / 6 h / Reflux; Inert atmosphere

6.1: pentamethylbenzene,; boron trichloride / dichloromethane / 0.55 h / -78 °C / Inert atmosphere

7.1: piperidine / ethanol / 3 h / 20 °C / Inert atmosphere

With piperidine; hydrogenchloride; sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; pentamethylbenzene,; boron trichloride; sodium hydride; toluene-4-sulfonic acid; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; toluene; mineral oil; tert-butyl alcohol; 7.1: |Aldol Condensation;
DOI:10.1016/j.tetlet.2019.151059