5-Methyltridecane

Base Information

• Chemical Name: 5-Methyltridecane
• CAS No.: 25117-31-1
• Molecular Formula: C14H30
• Molecular Weight: 198.392
• Hs Code.: 2901100000
• Mol file: 25117-31-1.mol

Synonyms:5-Methyltridecane

Chemical Property of 5-Methyltridecane

Chemical Property:

• Vapor Pressure: 0.043mmHg at 25°C
• Melting Point: -23.46°C (estimate)
• Refractive Index: 1.4161 (estimate)
• Boiling Point: 246.3°C at 760 mmHg
• Flash Point: 80.1°C
• PSA: 0.00000
• Density: 0.763g/cm³
• LogP: 5.56330

Purity/Quality:

99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Methyltridecane

There total 2 articles about 5-Methyltridecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

n-butyl magnesium bromide (693-03-8) + 2-bromodecane (39563-53-6,150927-20-1,150927-31-4) → decane (124-18-5) + 5-methyl-tridecane (25117-31-1) + 2-decene (20063-97-2,20348-51-0,6816-17-7)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; cobalt(II) chloride; lithium iodide; In tetrahydrofuran; at 10 ℃; for 1h; chemoselective reaction; Inert atmosphere;

DOI:10.1002/adsc.200800166

Reference yield:

1-Decene (872-05-9,17438-89-0,25189-70-2) + C12H27Al → 5-methyl-tridecane (25117-31-1) + 9-methyl nonadecane (13287-24-6)

Guidance literature:

With (-)-bis[(1-neomenthyl)indenyl]zirconium dichloride; In dichloromethane; at 23 ℃; for 20h; Product distribution;

DOI:10.1002/1521-3773(20020617)41:12<2141::AID-ANIE2141>3.0.CO;2-W

upstream raw materials:

1-Decene

n-butyl magnesium bromide

2-bromodecane