5-Hexenylboronic acid

Base Information

• Chemical Name: 5-Hexenylboronic acid
• CAS No.: 1072952-16-9
• Molecular Formula: C₆H₁₃BO₂
• Molecular Weight: 127.979
• Hs Code.: 2931900090
• Mol file: 1072952-16-9.mol

Synonyms:5-Hexenylboronic acid;Hex-5-en-1-ylboronic acid;Hex-5-enylboronic acid;5-Hexen-1-ylboronic acid

Chemical Property of 5-Hexenylboronic acid

Chemical Property:

• Melting Point: 67-73 °C
• Boiling Point: 241.5±33.0 °C(Predicted)
• PKA: 10.33±0.43(Predicted)
• PSA: 40.46000
• Density: 0.916±0.06 g/cm3(Predicted)
• LogP: 0.81550
• Storage Temp.: 2-8°C

Purity/Quality:

99% ^*data from raw suppliers

5-Hexenylboronic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 5-Hexenylboronic acid

Technology Process of 5-Hexenylboronic acid

There total 3 articles about 5-Hexenylboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-(hex-5-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane → hex-5-en-1-ylboronic acid (1072952-16-9)

Guidance literature:

With sodium periodate; ammonium acetate; In water; acetone; at 20 ℃; for 24h;

DOI:10.1016/j.chempr.2021.10.015

Reference yield:

Trimethyl borate (121-43-7,63156-11-6) + 6-Bromo-1-hexene (2695-47-8) → hex-5-en-1-ylboronic acid (1072952-16-9)

Guidance literature:

6-Bromo-1-hexene; With magnesium; In tetrahydrofuran; for 12h; Inert atmosphere; Reflux;

Trimethyl borate; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/acs.joc.6b01269

Reference yield:

6-Bromo-1-hexene (2695-47-8) → hex-5-en-1-ylboronic acid (1072952-16-9)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium; iodine / tetrahydrofuran / 20 °C

2: ammonium acetate; sodium periodate / water; acetone / 24 h / 20 °C

With sodium periodate; ammonium acetate; iodine; magnesium; In tetrahydrofuran; water; acetone;

DOI:10.1016/j.chempr.2021.10.015

upstream raw materials:

Trimethyl borate

6-Bromo-1-hexene

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