Technology Process of 1-Ethyloctylmethyl sulfide
There total 4 articles about 1-Ethyloctylmethyl sulfide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
decane-3-thiol;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at 0 - 20 ℃;
for 0.166667h;
Inert atmosphere;
methyl iodide;
In
tetrahydrofuran; hexane;
at 0 - 20 ℃;
for 0.333333h;
Inert atmosphere;
DOI:10.1021/jf506135c
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,N-dimethyl-formamide / 2 h / 80 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere
3.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / 0 - 20 °C / Inert atmosphere
3.2: 0.33 h / 0 - 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; n-butyllithium;
In
tetrahydrofuran; diethyl ether; hexane; N,N-dimethyl-formamide;
DOI:10.1021/jf506135c
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / 0 - 20 °C / Inert atmosphere
2.2: 0.33 h / 0 - 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; n-butyllithium;
In
tetrahydrofuran; diethyl ether; hexane;
DOI:10.1021/jf506135c
