1,3,5-TRIAZINO[1,2-A]BENZIMIDAZOL-2-AMINE, 4-METHYL-

Base Information

• Chemical Name: 1,3,5-TRIAZINO[1,2-A]BENZIMIDAZOL-2-AMINE, 4-METHYL-
• CAS No.: 78650-16-5
• Molecular Formula: C₁₀H₉N₅
• Molecular Weight: 199.215
• Hs Code.: 2933990090
• Mol file: 78650-16-5.mol

Synonyms:1,3,5-TRIAZINO[1,2-A]BENZIMIDAZOL-2-AMINE, 4-METHYL-;4-METHYL-1,3,5-TRIAZINO[1,2-A]BENZIMIDAZOL-2-AMINE;AKOS VGYB0001202;4-Methylbenzo[4,5]imidazo[1,2-a][1,3,5]triazin-2-amine

Chemical Property of 1,3,5-TRIAZINO[1,2-A]BENZIMIDAZOL-2-AMINE, 4-METHYL-

Chemical Property:

• PSA: 69.10000
• LogP: 1.74930

Purity/Quality:

97% ^*data from raw suppliers

4-methyl[1,3,5]triazino[1,2-a]benzimidazol-2-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3,5-TRIAZINO[1,2-A]BENZIMIDAZOL-2-AMINE, 4-METHYL-

There total 3 articles about 1,3,5-TRIAZINO[1,2-A]BENZIMIDAZOL-2-AMINE, 4-METHYL- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

2-guanidinobenzimidazole (5418-95-1) + Triethyl orthoacetate (78-39-7) → 2-amino-4-methyl-s-triazino[1,2-a]benzimidazole (78650-16-5)

Guidance literature:

In N,N-dimethyl-formamide; for 18h; Heating;

DOI:10.1002/jhet.5570430115

Reference yield: 30.0%

2-guanidinobenzimidazole (5418-95-1) + 2-methyl-4-oxo-4H-benzo[e][1,3]oxazinium perchlorate (54789-70-7) → 2-amino-4-methyl-s-triazino[1,2-a]benzimidazole (78650-16-5)

Guidance literature:

With sodium; In methanol; for 1h; Heating; 2;

DOI:10.1134/S1070428007100259

Reference yield:

1,2-diamino-benzene (95-54-5) → 2-amino-4-methyl-s-triazino[1,2-a]benzimidazole (78650-16-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 78 percent / conc. hydrochloric acid / H₂O / 1 h / Heating

2: 76 percent / dimethylformamide / 18 h / Heating

With hydrogenchloride; In water; N,N-dimethyl-formamide;

DOI:10.1002/jhet.5570430115

upstream raw materials:

2-guanidinobenzimidazole

Triethyl orthoacetate

1,2-diamino-benzene

2-methyl-4-oxo-4H-benzo[e][1,3]oxazinium perchlorate

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