2-(1H-1,2,3-Triazol-1-yl)...

Base Information

• Chemical Name: 2-(1H-1,2,3-Triazol-1-yl)...
• CAS No.: 1085458-53-2
• Molecular Formula: C9H7N3O2
• Molecular Weight: 189.173
• Hs Code.: 2933990090
• Mol file: 1085458-53-2.mol

Synonyms:2-(1H-1,2,3-Triazol-1-yl)...;2-(1H-1,2,3-Triazol-1-yl)benzoic acid

Chemical Property of 2-(1H-1,2,3-Triazol-1-yl)...

Chemical Property:

• PSA: 68.01000
• LogP: 0.96550

Purity/Quality:

97% ^*data from raw suppliers

2-(1H-1,2,3-Triazol-1-yl)benzoicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(1H-1,2,3-Triazol-1-yl)...

There total 6 articles about 2-(1H-1,2,3-Triazol-1-yl)... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

5-fluoro-2-iodobenzoic acid (52548-63-7) + 1 ,2,3-Triazole (288-36-8,288-35-7) → 2-(1H-1,2,3-triazol-1-yl)benzoic acid (1085458-53-2) + 5-fluoro-2-(2H-1,2,3-triazol-2-yl)benzoic acid (1186050-64-5)

Guidance literature:

5-fluoro-2-iodobenzoic acid; 1 ,2,3-Triazole; With caesium carbonate; trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; In N,N-dimethyl-formamide; at 100 ℃; for 0.166667h; Microwave ready vessel;

In water; Acidic conditions;

Reference yield:

1,2,3-triazole (288-36-8) + 2-Iodobenzoic acid (88-67-5) → 2-(2H-1,2,3-triazol-2-yl)benzoic acid (1001401-62-2) + 2-(1H-1,2,3-triazol-1-yl)benzoic acid (1085458-53-2)

Guidance literature:

With caesium carbonate; trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(l) iodide; In N,N-dimethyl-formamide; at 120 ℃; for 0.166667h; Microwave irradiation;

Reference yield:

2-Iodobenzoic acid (88-67-5) + 1 ,2,3-Triazole (288-36-8,288-35-7) → 2-(2H-1,2,3-triazol-2-yl)benzoic acid (1001401-62-2) + 2-(1H-1,2,3-triazol-1-yl)benzoic acid (1085458-53-2)

Guidance literature:

With copper(l) iodide; caesium carbonate; N,N’-trans-dimethyl cyclohexane-1,2-diamine; In N,N-dimethyl-formamide; at 120 ℃; for 0.166667h; Microwave irradiation;

upstream raw materials:

2-Iodobenzoic acid

1 ,2,3-Triazole

5-fluoro-2-iodobenzoic acid

1,2,3-triazole

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