4-(Hydrazinecarbonyl)benzamide

Base Information

• Chemical Name: 4-(Hydrazinecarbonyl)benzamide
• CAS No.: 22590-92-7
• Molecular Formula: C8H9N3O2
• Molecular Weight: 179.178
• Hs Code.: 2928000090
• DSSTox Substance ID: DTXSID30408616
• Mol file: 22590-92-7.mol

Synonyms:4-(hydrazinecarbonyl)benzamide;4-(hydrazinocarbonyl)benzamide;22590-92-7;SCHEMBL3780335;DTXSID30408616;MFCD03422938;AKOS000305344;VS-06554;BB 0260610;CS-0315030;FT-0678554

Chemical Property of 4-(Hydrazinecarbonyl)benzamide

Chemical Property:

• PSA: 98.21000
• Density: 1.32g/cm³
• LogP: 1.18050
• Storage Temp.: 2-8°C
• XLogP3: -0.5
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 2
• Exact Mass: 179.069476538
• Heavy Atom Count: 13
• Complexity: 209

Purity/Quality:

98%min ^*data from raw suppliers

4-(hydrazinocarbonyl)benzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1C(=O)N)C(=O)NN

Technology Process of 4-(Hydrazinecarbonyl)benzamide

There total 1 articles about 4-(Hydrazinecarbonyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

methyl-4-carbamoylbenzoate (6757-31-9) → 4-carbamoylbenzoic acid hydrazide (22590-92-7)

Guidance literature:

With hydrazine; In ethanol; at 130 ℃; for 0.5h; Microwave irradiation;

Reference yield: 39.0%

4-carbamoylbenzoic acid hydrazide (22590-92-7) + 7-[1-(tert-butoxycarbonyl)piperidin-4-yl]-5-oxo-4,5-dihydropyrazolo[1,5-a]pyrimidine-3-carboxylic acid → tert-butyl 4-(3-{[2-(4-carbamoylbenzoyl)hydrazino]carbonyl}-5-oxo-4,5-dihydropyrazolo[1,5-a]pyrimidin-7-yl)piperidine-1-carboxylate

Guidance literature:

With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield:

2-chloropyridine (109-09-1) + 4-carbamoylbenzoic acid hydrazide (22590-92-7) → C13H12N4O2

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (R)-(-)-1-[(S_P)-2-(dicyclohexylphosphino)ferrocenyl]ethyldi-tert-butylphosphine; sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 100 ℃; for 15h; chemoselective reaction;

DOI:10.1021/ol902868q

upstream raw materials:

methyl-4-carbamoylbenzoate

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