(3aS)-1-Benzoyl-1,2,3,3aα,8,8aα-hexahydro-3a,8-dimethylpyrrolo[2,3-b]indole

Base Information

Chemical Name:(3aS)-1-Benzoyl-1,2,3,3aα,8,8aα-hexahydro-3a,8-dimethylpyrrolo[2,3-b]indole
CAS No.:54833-65-7
Molecular Formula:C₁₉H₂₀N₂O
Molecular Weight:292.381
Hs Code.:
Mol file:54833-65-7.mol

Synonyms:(3aS)-1-Benzoyl-1,2,3,3aα,8,8aα-hexahydro-3a,8-dimethylpyrrolo[2,3-b]indole

Suppliers and Price of (3aS)-1-Benzoyl-1,2,3,3aα,8,8aα-hexahydro-3a,8-dimethylpyrrolo[2,3-b]indole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 3 raw suppliers

Chemical Property of (3aS)-1-Benzoyl-1,2,3,3aα,8,8aα-hexahydro-3a,8-dimethylpyrrolo[2,3-b]indole

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of (3aS)-1-Benzoyl-1,2,3,3aα,8,8aα-hexahydro-3a,8-dimethylpyrrolo[2,3-b]indole

There total 7 articles about (3aS)-1-Benzoyl-1,2,3,3aα,8,8aα-hexahydro-3a,8-dimethylpyrrolo[2,3-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 455-32-3
benzoyl fluoride

: 86724-46-1
N-(2-Isopropenyl-phenyl)-N-methyl-N'-trimethylsilanylmethyl-formamidine

: 54833-65-7,103303-62-4
(+/-)-1-benzoyl-3a,8-dimethyl-(3ar,8ac)-1,2,3,3a,8,8a-hexahydro-pyrrolo[2,3-b]indole

Guidance literature:: In acetonitrile; at 45 ℃; 2 h (reverse addition) than 12 h;
DOI:10.1016/S0040-4020(01)96709-2

Reference yield: 75.0%

: 4753-09-7
N-benzoyltryptamine

: 74-88-4
methyl iodide

: 54833-65-7,103303-62-4
(+/-)-1-benzoyl-3a,8-dimethyl-(3ar,8ac)-1,2,3,3a,8,8a-hexahydro-pyrrolo[2,3-b]indole

: C₁₈H₁₈N₂O

Guidance literature:: N-benzoyltryptamine; With potassium tert-butylate; In 1,4-dioxane; at 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

With triethyl borane; In tetrahydrofuran; 1,4-dioxane; for 0.5h; Schlenk technique; Inert atmosphere;

methyl iodide; In tetrahydrofuran; 1,4-dioxane; at 40 ℃; for 48h; Schlenk technique; Inert atmosphere;
DOI:10.1002/asia.201701151

Reference yield: 67.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 4753-09-7
N-benzoyltryptamine

: 74-88-4
methyl iodide

: 54833-65-7,103303-62-4
(+/-)-1-benzoyl-3a,8-dimethyl-(3ar,8ac)-1,2,3,3a,8,8a-hexahydro-pyrrolo[2,3-b]indole

Guidance literature:: N-benzoyltryptamine; With potassium tert-butylate; In 1,4-dioxane; at 20 ℃; for 0.5h; Schlenk technique; Inert atmosphere;

With triethyl borane; In tetrahydrofuran; 1,4-dioxane; for 0.5h; Schlenk technique; Inert atmosphere;

formaldehyd; methyl iodide; Further stages;
DOI:10.1002/asia.201701151