1,3-DICHLORO-5-BROMOISOQUINOLINE

Base Information

Chemical Name:1,3-DICHLORO-5-BROMOISOQUINOLINE
CAS No.:1215767-89-7
Molecular Formula:C9H4BrCl2N
Molecular Weight:276.94
Hs Code.:
Mol file:1215767-89-7.mol

Synonyms:1,3-DICHLORO-5-BROMOISOQUINOLINE

Suppliers and Price of 1,3-DICHLORO-5-BROMOISOQUINOLINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Bromo-1,3-dichloroisoquinoline
100mg
$ 200.00

Crysdot
5-Bromo-1,3-dichloroisoquinoline 95+%
1g
$ 581.00

Crysdot
5-Bromo-1,3-dichloroisoquinoline 95+%
5g
$ 1748.00

Chemenu
5-Bromo-1,3-dichloroisoquinoline 95%
5g
$ 1561.00

Chemenu
5-Bromo-1,3-dichloroisoquinoline 95%
1g
$ 514.00

Alichem
5-Bromo-1,3-dichloroisoquinoline
1g
$ 454.30

Alichem
5-Bromo-1,3-dichloroisoquinoline
5g
$ 1264.80

AK Scientific
1,3-DICHLORO-5-BROMOISOQUINOLINE
1g
$ 622.40

AK Scientific
1,3-DICHLORO-5-BROMOISOQUINOLINE
250mg
$ 335.60

Total 13 raw suppliers

Chemical Property of 1,3-DICHLORO-5-BROMOISOQUINOLINE

Chemical Property:

PSA：12.89000
LogP:4.30410
Storage Temp.:Inert atmosphere,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

5-Bromo-1,3-dichloroisoquinoline ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-DICHLORO-5-BROMOISOQUINOLINE

There total 3 articles about 1,3-DICHLORO-5-BROMOISOQUINOLINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 7742-73-6
1,3-dichloroisoquinoline

: 1215767-89-7
5-bromo-1,3-dichloroisoquinoline

Guidance literature:: With N-Bromosuccinimide; sulfuric acid; In acetonitrile; at 20 ℃; for 72h;
DOI:10.1002/chem.202001572

Reference yield:

: 4-bromo-2-(hydroxyimino)-2,3-dihydro-1H-inden-1-one

: 1215767-89-7
5-bromo-1,3-dichloroisoquinoline

Guidance literature:: With N,N-dimethyl-formamide; trichlorophosphate; at 120 ℃; for 0.75h; Sealed tube; Cooling with ice; Sonication;

Reference yield:

: 15115-60-3
4-bromo-2,3-dihydroinden-1-one

: 1215767-89-7
5-bromo-1,3-dichloroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; ethyl nitrite / diethyl ether; ethanol; dichloromethane / 4 h / 0 - 20 °C

2: trichlorophosphate; N,N-dimethyl-formamide / 0.75 h / 120 °C / Sealed tube; Cooling with ice; Sonication

With hydrogenchloride; ethyl nitrite; N,N-dimethyl-formamide; trichlorophosphate; In diethyl ether; ethanol; dichloromethane;