N-(2-AMinoethyl)acrylaMide hydrochloride

Base Information

• Chemical Name: N-(2-AMinoethyl)acrylaMide hydrochloride
• CAS No.: 54641-27-9
• Molecular Formula: C5H11ClN2O
• Molecular Weight: 150.60664
• Hs Code.: 2924199090
• Mol file: 54641-27-9.mol

Synonyms:N-(2-aminoethyl)prop-2-enamide hydrochloride

Chemical Property of N-(2-AMinoethyl)acrylaMide hydrochloride

Chemical Property:

• PSA: 58.61000
• LogP: 1.58990
• Storage Temp.: Inert atmosphere,Store in freezer, under -20°C

Purity/Quality:

97% ^*data from raw suppliers

N-(2-aminoethyl)acrylamidehydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(2-AMinoethyl)acrylaMide hydrochloride

There total 2 articles about N-(2-AMinoethyl)acrylaMide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl (2-acrylamidoethyl)carbamate (165196-44-1) → N-(2-aminoethyl)prop-2-enamide hydrochloride (54641-27-9)

Guidance literature:

With hydrogenchloride; In dichloromethane; at 20 ℃; for 3h; Schlenk technique; Inert atmosphere;

DOI:10.1055/s-0033-1338614

Reference yield:

ethylenediamine (107-15-3,85404-18-8) + acryloyl chloride (814-68-6,25189-84-8) → N-(2-aminoethyl)prop-2-enamide hydrochloride (54641-27-9)

Guidance literature:

ethylenediamine; With hydrogenchloride; In water; pH=8.5;

acryloyl chloride; In chloroform; water; at 20 ℃; for 2h;

Reference yield:

N-(2-aminoethyl)prop-2-enamide hydrochloride (54641-27-9) → N-[beta-aminoethyl]acrylamide (23918-29-8)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 1,1'-carbonyldiimidazole / dichloromethane / 2 h / 20 °C

1.2: 20 °C

2.1: trifluoroacetic acid / dichloromethane / 20 °C

3.1: γ-glutamyl transpeptidase / water-d2 / 37 °C / pH 7.4 / Enzymatic reaction

With γ-glutamyl transpeptidase; 1,1'-carbonyldiimidazole; trifluoroacetic acid; In dichloromethane; water-d2;

upstream raw materials:

tert-butyl (2-acrylamidoethyl)carbamate

ethylenediamine

acryloyl chloride

Downstream raw materials:

N-[beta-aminoethyl]acrylamide

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