Benzoic acid, 4-(2-methyl-3-oxopropyl)-, methyl ester, (S)- (9CI)

Base Information

Chemical Name:Benzoic acid, 4-(2-methyl-3-oxopropyl)-, methyl ester, (S)- (9CI)
CAS No.:204587-79-1
Molecular Formula:C₁₂H₁₄O₃
Molecular Weight:206.241
Hs Code.:
Mol file:204587-79-1.mol

Synonyms:Benzoic acid, 4-(2-methyl-3-oxopropyl)-, methyl ester, (S)- (9CI)

Suppliers and Price of Benzoic acid, 4-(2-methyl-3-oxopropyl)-, methyl ester, (S)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid, 4-(2-methyl-3-oxopropyl)-, methyl ester, (S)- (9CI)

Chemical Property:

PSA：43.37000
LogP:1.85070

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzoic acid, 4-(2-methyl-3-oxopropyl)-, methyl ester, (S)- (9CI)

There total 3 articles about Benzoic acid, 4-(2-methyl-3-oxopropyl)-, methyl ester, (S)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 170955-25-6
(S)-(-)-3-(4-methoxycarbonyl)phenyl-2-methyl-1-propanol

: 204587-79-1
4-((S)-2-Methyl-3-oxo-propyl)-benzoic acid methyl ester

Guidance literature:: With Celite; pyridinium chlorochromate; In dichloromethane; for 0.5h;
DOI:10.1002/ijch.199600025

Reference yield:

: 2417-72-3
Methyl 4-(bromomethyl)benzoate

: 204587-79-1
4-((S)-2-Methyl-3-oxo-propyl)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LDA / 1.) THF, -78 deg C, 30 min, 2.) THF, -20 deg C, 5 h

2: 90 percent / NaBH₄ / methanol / 0.5 h / 0 °C

3: pyridinium chlorochromate, Celite / CH₂Cl₂ / 0.5 h

With sodium tetrahydroborate; Celite; pyridinium chlorochromate; lithium diisopropyl amide; In methanol; dichloromethane;
DOI:10.1002/ijch.199600025

Reference yield:

: 4-[(S)-2-Methyl-3-((4R,5S)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-3-oxo-propyl]-benzoic acid methyl ester

: 204587-79-1
4-((S)-2-Methyl-3-oxo-propyl)-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaBH₄ / methanol / 0.5 h / 0 °C

2: pyridinium chlorochromate, Celite / CH₂Cl₂ / 0.5 h

With sodium tetrahydroborate; Celite; pyridinium chlorochromate; In methanol; dichloromethane;
DOI:10.1002/ijch.199600025