2-[(4-methyl-5-phenyl-4H-1,2,4-triazol-3-yl)thio]acetohydrazide

Base Information

• Chemical Name: 2-[(4-methyl-5-phenyl-4H-1,2,4-triazol-3-yl)thio]acetohydrazide
• CAS No.: 120873-48-5
• Molecular Formula: C₁₁H₁₃N₅OS
• Molecular Weight: 263.323
• Hs Code.: 2933990090
• Mol file: 120873-48-5.mol

Synonyms:2-[(4-methyl-5-phenyl-4H-1,2,4-triazol-3-yl)thio]acetohydrazide

Chemical Property of 2-[(4-methyl-5-phenyl-4H-1,2,4-triazol-3-yl)thio]acetohydrazide

Chemical Property:

• PSA: 111.13000
• LogP: 1.65530

Purity/Quality:

97% ^*data from raw suppliers

2-((4-Methyl-5-phenyl-4H-1,2,4-triazol-3-yl)thio)acetohydrazide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-[(4-methyl-5-phenyl-4H-1,2,4-triazol-3-yl)thio]acetohydrazide

There total 4 articles about 2-[(4-methyl-5-phenyl-4H-1,2,4-triazol-3-yl)thio]acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H15N3O2S → 2-[(4-methyl-5-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetohydrazide (120873-48-5)

Guidance literature:

With hydrazine hydrate; In ethanol;

DOI:10.3184/174751917X14815427219040

Reference yield:

benzoic acid hydrazide (613-94-5) → 2-[(4-methyl-5-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetohydrazide (120873-48-5)

Guidance literature:

Multi-step reaction with 4 steps

1: ethanol

2: sodium hydroxide / ethanol

3: potassium carbonate / acetone

4: hydrazine hydrate / ethanol

With potassium carbonate; hydrazine hydrate; sodium hydroxide; In ethanol; acetone;

DOI:10.3184/174751917X14815427219040

Reference yield:

1-(phenyl)carbonyl-4-(methyl)thiosemicarbazide (58064-65-6) → 2-[(4-methyl-5-phenyl-4H-1,2,4-triazol-3-yl)sulfanyl]acetohydrazide (120873-48-5)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol

2: potassium carbonate / acetone

3: hydrazine hydrate / ethanol

With potassium carbonate; hydrazine hydrate; sodium hydroxide; In ethanol; acetone;

DOI:10.3184/174751917X14815427219040

upstream raw materials:

benzoic acid hydrazide

1-(phenyl)carbonyl-4-(methyl)thiosemicarbazide

3-mercapto-4-methyl-5-phenyl-1,2,4(4H)-triazole

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