2-Methyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline

Base Information

Chemical Name:2-Methyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline
CAS No.:850689-28-0
Molecular Formula:C13H20BNO2
Molecular Weight:233.11
Hs Code.:
Mol file:850689-28-0.mol

Synonyms:2-Methyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline

Suppliers and Price of 2-Methyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Amino-4-methylphenylboronicAcidPinacolEster
50mg
$ 45.00

AOBChem
3-Amino-4-methylphenylboronicacidpinacolester 97%
25g
$ 1202.00

Total 9 raw suppliers

Chemical Property of 2-Methyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline

Chemical Property:

PSA：44.48000
LogP:2.45760

Purity/Quality:

99% ^*data from raw suppliers

3-Amino-4-methylphenylboronicAcidPinacolEster ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Methyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline

There total 6 articles about 2-Methyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1072945-06-2
4,4,5,5-tetramethyl-2-(4-methyl-3-nitrophenyl)-1,3,2-dioxaborolane

: 850689-28-0
2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In methanol; at 20 ℃; for 4h; under 760.051 Torr;
DOI:10.1021/jo402618r

Reference yield: 72.0%

: 83863-33-6
5-iodo-o-toluidine

: 73183-34-3
bis(pinacol)diborane

: 850689-28-0
2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

Guidance literature:: With 10H-phenothiazine; caesium carbonate; In acetonitrile; for 48h; Irradiation; Sealed tube; Inert atmosphere;
DOI:10.1021/jacs.9b12519

Reference yield: 51.1%

: 39478-78-9
5-bromo-2-methylaniline

: 73183-34-3
bis(pinacol)diborane

: 850689-28-0
2-methyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)aniline

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; for 3h; Inert atmosphere; Reflux;
DOI:10.1021/acs.organomet.0c00211