tert-Butyl 2-(1-iminoethyl)hydrazinecarboxylate

Base Information

• Chemical Name: tert-Butyl 2-(1-iminoethyl)hydrazinecarboxylate
• CAS No.: 851535-08-5
• Molecular Formula: C7H15N3O2
• Molecular Weight: 173.215
• Hs Code.: 2924297099
• Mol file: 851535-08-5.mol

Synonyms:tert-Butyl 2-(1-iminoethyl)hydrazinecarboxylate;tert-butyl2-(1-iminoethyl)hydrazine-1-carboxylate

Chemical Property of tert-Butyl 2-(1-iminoethyl)hydrazinecarboxylate

Chemical Property:

• PKA: 8.21±0.43(Predicted)
• PSA: 74.21000
• Density: 1.10±0.1 g/cm3(Predicted)
• LogP: 1.89440

Purity/Quality:

97% ^*data from raw suppliers

N-Boc-2-(1-Iminoethyl)hydrazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tert-Butyl 2-(1-iminoethyl)hydrazinecarboxylate

There total 1 articles about tert-Butyl 2-(1-iminoethyl)hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

t-butoxycarbonylhydrazine (870-46-2) + ethyl acetimidate hydrochloride (2208-07-3) → tert-butyl 2-ethanimidoylhydrazinecarboxylate (851535-08-5)

Guidance literature:

With sodium hydroxide; In ethanol; at 0 - 70 ℃; for 2.5h;

Reference yield: 100.0%

2-bromo-2'-fluoroacetophenone (655-15-2) + tert-butyl 2-ethanimidoylhydrazinecarboxylate (851535-08-5) → tert-butyl [4-(2-fluorophenyl)-2-methyl-1H-imidazol-1-yl]carbamate

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In 2-methyltetrahydrofuran; acetonitrile; for 18h; Reflux;

upstream raw materials:

t-butoxycarbonylhydrazine

ethyl acetimidate hydrochloride

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