o-Pentyloxyphenol

Base Information

• Chemical Name: o-Pentyloxyphenol
• CAS No.: 58761-99-2
• Molecular Formula: C11H16O2
• Molecular Weight: 180.247
• Mol file: 58761-99-2.mol

Synonyms:o-Pentyloxyphenol

Chemical Property of o-Pentyloxyphenol

Chemical Property:

• Boiling Point: 104 - 106 °C (4 mmHg)
• PSA: 29.46000
• LogP: 2.96120

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of o-Pentyloxyphenol

There total 4 articles about o-Pentyloxyphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1-Bromopentane (110-53-2) + benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 2-(n-pentyloxy)-phenol (58761-99-2)

Guidance literature:

With tetrabutylammomium bromide; potassium carbonate; potassium iodide; In ethanol; for 24h; Reflux;

DOI:10.1039/c6ce00365f

Reference yield:

benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 2-(n-pentyloxy)-phenol (58761-99-2)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/ja01342a053

Reference yield:

1-bromo-hexane (111-25-1) + benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 2-(n-pentyloxy)-phenol (58761-99-2) + 1,2-bis(pentyloxy)benzene (142947-21-5)

Guidance literature:

With potassium carbonate; In ethanol;

DOI:10.1080/15421400903051093

upstream raw materials:

benzene-1,2-diol

1-Bromopentane

1-bromo-hexane

Downstream raw materials:

5-methylthio-2-(n-pentyloxy)-phenol

4-methylthio-2-(n-pentyloxy)-phenol

2,3,6,7,10,11-hexakis(pentyloxy)triphenylene

2-hydroxy-3,6,7,10,11-pentapentyloxytriphenylene

Refernces

• 1、 Zhao,Bai,Hu,Wang,Shimizu. "Synthesis of triphenylene discotic liquid crystal dimers: Click chemistry as an efficient tool". scheme or table. p. 77 - 88. Retrieved 2011/08/07.