Technology Process of 5-Iodonaphthalene-1-carboxylic acid
There total 3 articles about 5-Iodonaphthalene-1-carboxylic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
jones reagent;
In
acetone;
for 0.283333h;
Yield given;
DOI:10.1021/jo00008a059
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1) tert-BuLi, 2) tetramethylethylenediamine / 1) ether, -78 deg C up to 5 deg C, 6.5 h, 2) up to room temp., 17 h
2: Jones reagent / acetone / 0.28 h
With
jones reagent; N,N,N,N,-tetramethylethylenediamine; tert.-butyl lithium;
In
acetone;
DOI:10.1021/jo00008a059
- Guidance literature:
-
Diazotization.man setzt die Diazoverbindung mit Kaliumjodid um;