5-Amino-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose

Base Information

Chemical Name:5-Amino-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose
CAS No.:109681-00-7
Molecular Formula:C₂₈H₃₁NO₅
Molecular Weight:461.558
Hs Code.:
Mol file:109681-00-7.mol

Synonyms:5-Amino-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose;5-AMino-5-deoxy-1,2-O-(1-Methylethylidene)-6-O-(triphenylMethyl)-α-D-galactofuranose

Suppliers and Price of 5-Amino-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Amino-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose
25mg
$ 1320.00

Medical Isotopes, Inc.
5-Amino-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose
5 mg
$ 845.00

American Custom Chemicals Corporation
5-AMINO-5-DEOXY-1,2-O-ISOPROPYLIDENE-6-O-TRITYL-A-D-GALACTOFURANOSE 95.00%
5MG
$ 497.33

Total 3 raw suppliers

Chemical Property of 5-Amino-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose

Chemical Property:

PSA：83.17000
LogP:4.26000
Solubility.:Chloroform, Methanol

Purity/Quality:

95% ^*data from raw suppliers

5-Amino-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Amino-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose

There total 7 articles about 5-Amino-5-deoxy-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38166-65-3
3-O-acetyl-1,2:5,6-di-O-isopropylidene-α-D-galactofuranose

: 109681-00-7
5-amino-5-deoxy-1,2-O-isoproylidene-6-O-trityl-α-D-galactofuranose

Guidance literature:: Multi-step reaction with 6 steps

1: 50percent aq. AcOH / 5 h / Ambient temperature; concentrated at 25 deg C

2: 98 percent / pyridine / 7 h / 70 °C

3: 95 percent / pyridinium dichromate, Ac₂O / CH₂Cl₂ / 1 h / Heating

4: 96 percent / hydroxylammonium chloride, KHCO₃ / methanol / Heating

5: 0.01 M NaOMe / methanol

6: hydrogen / Raney-Ni

With pyridine; dipyridinium dichromate; hydroxylamine hydrochloride; hydrogen; sodium methylate; acetic anhydride; potassium hydrogencarbonate; acetic acid; nickel; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)90138-1

Reference yield:

: 109680-98-0
3-O-acetyl-1,2-O-isopropylidene-6-O-trityl-β-L-arabino-hexofuranos-5-ulose

: 109681-00-7
5-amino-5-deoxy-1,2-O-isoproylidene-6-O-trityl-α-D-galactofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / hydroxylammonium chloride, KHCO₃ / methanol / Heating

2: 0.01 M NaOMe / methanol

3: hydrogen / Raney-Ni

With hydroxylamine hydrochloride; hydrogen; sodium methylate; potassium hydrogencarbonate; nickel; In methanol;
DOI:10.1016/S0008-6215(00)90138-1

Reference yield:

: 109680-97-9
3-O-acetyl-1,2-O-isopropylidene-6-O-trityl-α-D-galactofuranose

: 109681-00-7
5-amino-5-deoxy-1,2-O-isoproylidene-6-O-trityl-α-D-galactofuranose

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / pyridinium dichromate, Ac₂O / CH₂Cl₂ / 1 h / Heating

2: 96 percent / hydroxylammonium chloride, KHCO₃ / methanol / Heating

3: 0.01 M NaOMe / methanol

4: hydrogen / Raney-Ni

With dipyridinium dichromate; hydroxylamine hydrochloride; hydrogen; sodium methylate; acetic anhydride; potassium hydrogencarbonate; nickel; In methanol; dichloromethane;
DOI:10.1016/S0008-6215(00)90138-1