BZL-ILE-OME HCL

Base Information

• Chemical Name: BZL-ILE-OME HCL
• CAS No.: 209325-69-9
• Molecular Formula: C14H22ClNO2
• Molecular Weight: 235.326
• Mol file: 209325-69-9.mol

Synonyms:N-ALPHA-BENZYL-L-ISOLEUCINE METHYL ESTER HYDROCHLORID;N-ALPHA-BENZYL-L-ISOLEUCINE METHYL ESTER HYDROCHLORIDE;BZL-L-ILE-OME HCL;BZL-ILE-OME HCL;BENZYL-L-ISOLEUCINE METHYL ESTER HYDROCHLORIDE

Chemical Property of BZL-ILE-OME HCL

Chemical Property:

• PSA: 38.33000
• LogP: 2.75480

Purity/Quality:

98%Min ^*data from raw suppliers

Benzyl-L-isoleucine methyl ester hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BZL-ILE-OME HCL

There total 6 articles about BZL-ILE-OME HCL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2S,3S)-3-Methyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-pentanoic acid methyl ester (40216-73-7) → methyl (2S,3S)-2-(benzylamino)-3-methylpentanoate (209325-69-9)

Guidance literature:

With sodium tetrahydroborate; In methanol; for 0.5h;

DOI:10.1016/S0040-4039(02)00352-0

Reference yield:

methyl L-isoleucinate hydrochloride (18598-74-8) → methyl (2S,3S)-2-(benzylamino)-3-methylpentanoate (209325-69-9)

Guidance literature:

Multi-step reaction with 2 steps

1: TEA; MgSO₄ / tetrahydrofuran / 5 h / 20 °C

2: NaBH₄ / methanol / 0.5 h

With sodium tetrahydroborate; TEA; magnesium sulfate; In tetrahydrofuran; methanol;

DOI:10.1016/S0040-4039(02)00352-0

Reference yield:

benzaldehyde (100-52-7) → methyl (2S,3S)-2-(benzylamino)-3-methylpentanoate (209325-69-9)

Guidance literature:

Multi-step reaction with 2 steps

1: TEA; MgSO₄ / tetrahydrofuran / 5 h / 20 °C

2: NaBH₄ / methanol / 0.5 h

With sodium tetrahydroborate; TEA; magnesium sulfate; In tetrahydrofuran; methanol;

DOI:10.1016/S0040-4039(02)00352-0

upstream raw materials:

diazomethane

(2S,3S)-2-(benzylamino)-3-methylpentanoic acid

(2S,3S)-3-Methyl-2-{[1-phenyl-meth-(E)-ylidene]-amino}-pentanoic acid methyl ester

methyl L-isoleucinate hydrochloride

Downstream raw materials:

(2S,3S)-2-(benzylamino)-3-methylpentan-1-ol

tert-butyl 2-allyl-2-(benzyl((2S,3S)-1-methoxy-3-methyl-1-oxopentan-2-yl)carbamoyl)hydrazine-1-carboxylate

(3S,6R)-2-benzyl-3-((S)-sec-butyl)-6-methoxyhexahydropyridazino[1,2-a][1,2,4]triazine-1,4-dione

(S)-2-allyl-4-benzyl-5-((S)-sec-butyl)-1,2,4-triazinane-3,6-dione

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