(15β)-20,21-Didehydro-16β-(hydroxymethyl)-18,19-secoyohimban-19-oic acid methyl ester

Base Information

Chemical Name:(15β)-20,21-Didehydro-16β-(hydroxymethyl)-18,19-secoyohimban-19-oic acid methyl ester
CAS No.:5552-25-0
Molecular Formula:
Molecular Weight:354.44
Hs Code.:
Mol file:5552-25-0.mol

Synonyms:(15β)-20,21-Didehydro-16β-(hydroxymethyl)-18,19-secoyohimban-19-oic acid methyl ester;Tetrahydrovallesiachotamine

Suppliers and Price of (15β)-20,21-Didehydro-16β-(hydroxymethyl)-18,19-secoyohimban-19-oic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (15β)-20,21-Didehydro-16β-(hydroxymethyl)-18,19-secoyohimban-19-oic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (15β)-20,21-Didehydro-16β-(hydroxymethyl)-18,19-secoyohimban-19-oic acid methyl ester

There total 6 articles about (15β)-20,21-Didehydro-16β-(hydroxymethyl)-18,19-secoyohimban-19-oic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5523-37-5,34384-71-9,93862-63-6,93862-64-7
(+/-)-vallesiachotaminen

: 5552-25-0,34384-68-4
tetrahydrovallesiachotamine

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / ethanol / 3 h

2: H₂ / PtO₂ / ethanol / 12 h

With sodium tetrahydroborate; hydrogen; platinum(IV) oxide; In ethanol;
DOI:10.1016/0040-4020(82)85081-3

Reference yield:

: 5523-37-5,34384-71-9,93862-63-6,93862-64-7
(+/-)-vallesiachotaminen

: 5552-25-0,34384-68-4
tetrahydrovallesiachotamine

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / ethanol / 3 h

2: H₂ / PtO₂ / ethanol / 12 h

With sodium tetrahydroborate; hydrogen; platinum(IV) oxide; In ethanol;
DOI:10.1016/0040-4020(82)85081-3

Reference yield:

: 5523-49-9,34384-66-2,93862-69-2,93894-89-4
dihydrovallesiachotamine

: (2S,12bS)-2-sec-Butyl-1,2,6,7,12,12b-hexahydro-indolo[2,3-a]quinolizine-3-carboxylic acid methyl ester

: 5552-25-0,34384-68-4
tetrahydrovallesiachotamine

: 5552-25-0,34384-68-4
tetrahydrovallesiachotamine

Guidance literature:: With hydrogen; platinum(IV) oxide; In ethanol; for 12h; Yield given. Yields of byproduct given;
DOI:10.1016/0040-4020(82)85081-3