1,3,3a,6,7,7a-Hexahydro-2-(4-methoxyphenyl)-3a,6-epoxy-2H-isoindole

Base Information

• Chemical Name: 1,3,3a,6,7,7a-Hexahydro-2-(4-methoxyphenyl)-3a,6-epoxy-2H-isoindole
• CAS No.: 17960-79-1
• Molecular Formula: C15H17NO2
• Molecular Weight: 0
• Mol file: 17960-79-1.mol

Synonyms:1,2,3,6,7,7a-Hexahydro-2-(4-methoxyphenyl)-3a,6-epoxy-3aH-isoindole;1,3,3a,6,7,7a-Hexahydro-2-(4-methoxyphenyl)-3a,6-epoxy-2H-isoindole

Chemical Property of 1,3,3a,6,7,7a-Hexahydro-2-(4-methoxyphenyl)-3a,6-epoxy-2H-isoindole

Chemical Property:

• Melting Point: 138 - 139 °C (petroleum ether)
• PSA: 21.70000
• LogP: 2.29390

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of 1,3,3a,6,7,7a-Hexahydro-2-(4-methoxyphenyl)-3a,6-epoxy-2H-isoindole

There total 2 articles about 1,3,3a,6,7,7a-Hexahydro-2-(4-methoxyphenyl)-3a,6-epoxy-2H-isoindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N-(furan-2-ylmethyl)-4-methoxybenzenamine (17377-97-8) + allyl bromide (106-95-6) → 2-(4-methoxy-phenyl)-1,2,3,6,7,7a-hexahydro-3a,6-epioxido-isoindole (17960-79-1)

Guidance literature:

With N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate; In benzene; at 80 ℃; for 7h; Heating;

Reference yield:

→ 2-(4-methoxy-phenyl)-1,2,3,6,7,7a-hexahydro-3a,6-epioxido-isoindole (17960-79-1)

Guidance literature:

Allylaryl(2-furfuryl)amin(IV),intramolekulare <4+2>-Cycloaddition;

Reference yield: 65.0%

2-(4-methoxy-phenyl)-1,2,3,6,7,7a-hexahydro-3a,6-epioxido-isoindole (17960-79-1) + N-phenylsulfinylamine (222851-56-1) → C21H22N2O3S (110108-38-8)

Guidance literature:

In benzene; for 50h; Ambient temperature;

upstream raw materials:

N-(furan-2-ylmethyl)-4-methoxybenzenamine

allyl bromide

Downstream raw materials:

C₂₁H₂₂N₂O₃S

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