25-Acetyl-15,16-dimethoxy-22α-methyl-4,25-secoobscurinervan-4-one

Base Information

Chemical Name:25-Acetyl-15,16-dimethoxy-22α-methyl-4,25-secoobscurinervan-4-one
CAS No.:54658-10-5
Molecular Formula:C26H34N2O6
Molecular Weight:470.56
Hs Code.:
Mol file:54658-10-5.mol

Synonyms:25-Acetyl-15,16-dimethoxy-22α-methyl-4,25-secoobscurinervan-4-one

Suppliers and Price of 25-Acetyl-15,16-dimethoxy-22α-methyl-4,25-secoobscurinervan-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 25-Acetyl-15,16-dimethoxy-22α-methyl-4,25-secoobscurinervan-4-one

Chemical Property:

PSA：77.54000
LogP:2.69450

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 25-Acetyl-15,16-dimethoxy-22α-methyl-4,25-secoobscurinervan-4-one

There total 4 articles about 25-Acetyl-15,16-dimethoxy-22α-methyl-4,25-secoobscurinervan-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7168-67-4
obscurinervidine

: 54658-10-5
Dihydro-obscurinervidinolon-acetat

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd-C / ethyl acetate

2: LiAlH₄ / diethyl ether / Heating

3: K₂CO₃

4: DCC, DMSO, H₃PO₄

With lithium aluminium tetrahydride; phosphoric acid; hydrogen; potassium carbonate; dimethyl sulfoxide; dicyclohexyl-carbodiimide; palladium on activated charcoal; In diethyl ether; ethyl acetate;
DOI:10.1021/ja01066a031

Reference yield:

: 6887-30-5
obscurinervidine

: 54658-10-5
Dihydro-obscurinervidinolon-acetat

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether / Heating

2: K₂CO₃

3: DCC, DMSO, H₃PO₄

With lithium aluminium tetrahydride; phosphoric acid; potassium carbonate; dimethyl sulfoxide; dicyclohexyl-carbodiimide; In diethyl ether;
DOI:10.1021/ja01066a031