15,16-Dimethoxy-22α-methyl-4,25-secoobscurinervan-4β-ol

Base Information

Chemical Name:15,16-Dimethoxy-22α-methyl-4,25-secoobscurinervan-4β-ol
CAS No.:54678-26-1
Molecular Formula:C24H34N2O5
Molecular Weight:430.54
Hs Code.:
Mol file:54678-26-1.mol

Synonyms:15,16-Dimethoxy-22α-methyl-4,25-secoobscurinervan-4β-ol;Dihydroobscurinervidinediol

Suppliers and Price of 15,16-Dimethoxy-22α-methyl-4,25-secoobscurinervan-4β-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 15,16-Dimethoxy-22α-methyl-4,25-secoobscurinervan-4β-ol

Chemical Property:

Boiling Point:630.7±55.0 °C(Predicted)
PKA:14.42±0.60(Predicted)
Density:1.35±0.1 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 15,16-Dimethoxy-22α-methyl-4,25-secoobscurinervan-4β-ol

There total 2 articles about 15,16-Dimethoxy-22α-methyl-4,25-secoobscurinervan-4β-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7168-67-4
obscurinervidine

: 54678-26-1
15,16-dimethoxy-5'α-methyl-5',6'-dihydro-[1,4]oxazino[4',3',2':1,18,17]aspidospermidine-4β,21-diol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / Pd-C / ethyl acetate

2: LiAlH₄ / diethyl ether / Heating

With lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; ethyl acetate;
DOI:10.1021/ja01066a031

Reference yield:

: 6887-30-5
obscurinervidine

: 54678-26-1
15,16-dimethoxy-5'α-methyl-5',6'-dihydro-[1,4]oxazino[4',3',2':1,18,17]aspidospermidine-4β,21-diol

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; Heating;
DOI:10.1021/ja01066a031

Reference yield:

: 54678-26-1
15,16-dimethoxy-5'α-methyl-5',6'-dihydro-[1,4]oxazino[4',3',2':1,18,17]aspidospermidine-4β,21-diol

: 54658-10-5
Dihydro-obscurinervidinolon-acetat

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃

2: DCC, DMSO, H₃PO₄

With phosphoric acid; potassium carbonate; dimethyl sulfoxide; dicyclohexyl-carbodiimide;
DOI:10.1021/ja01066a031