Dansyllysine

Base Information

Chemical Name:Dansyllysine
CAS No.:1101-84-4
Molecular Formula:C18H25 N3 O4 S
Molecular Weight:379.47
Hs Code.:2935009090
UNII:EFF64524YR
DSSTox Substance ID:DTXSID20149142
Nikkaji Number:J375.981D
Wikidata:Q27095420
Metabolomics Workbench ID:149109
Mol file:1101-84-4.mol

Synonyms:dansyllysine;dns-lysine;N(epsilon)-dansyl-L-lysine

Suppliers and Price of Dansyllysine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Dansyllysine

Chemical Property:

Vapor Pressure:5.82E-15mmHg at 25°C
Boiling Point:594.1°Cat760mmHg
Flash Point:313.1°C
PSA：121.11000
Density:1.293g/cm³
LogP:3.93830
Storage Temp.:−20°C
XLogP3:-0.1
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:9
Exact Mass:379.15657746
Heavy Atom Count:26
Complexity:561

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Canonical SMILES:CN(C)C1=CC=CC2=C1C=CC=C2S(=O)(=O)NCCCCC(C(=O)O)N
Isomeric SMILES:CN(C)C1=CC=CC2=C1C=CC=C2S(=O)(=O)NCCCC[C@@H](C(=O)O)N

Technology Process of Dansyllysine

There total 9 articles about Dansyllysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 827021-74-9
N^(α)-benzyloxycarbonyl-N^(ε)-5-(dimethylamino)naphthalene-1-sulfonyl-L-lysine benzyl ester

: 1101-84-4
N^(ε)-5-(dimethylamino)naphthalene-1-sulfonyl-L-lysine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; for 6h;
DOI:10.1021/ja046164n

Reference yield:

: 605-65-2
5-(dimethylamino)naphth-1-ylsulfonyl chloride

: 1101-84-4
N^(ε)-5-(dimethylamino)naphthalene-1-sulfonyl-L-lysine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / triethylamine / CH₂Cl₂ / 6.5 h / 0 - 20 °C

2: 100 percent / H₂ / Pd/C / methanol / 6 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja046164n

Reference yield:

: 5591-94-6
N^(α)-benzyloxycarbonyl-L-lysine benzyl ester

: 1101-84-4
N^(ε)-5-(dimethylamino)naphthalene-1-sulfonyl-L-lysine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / triethylamine / CH₂Cl₂ / 6.5 h / 0 - 20 °C

2: 100 percent / H₂ / Pd/C / methanol / 6 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja046164n