2-Amino-6-bromobenzenethiol

Base Information

• Chemical Name: 2-Amino-6-bromobenzenethiol
• CAS No.: 824932-42-5
• Molecular Formula: C₆H₆BrNS
• Molecular Weight: 204.09
• Mol file: 824932-42-5.mol

Synonyms:2-Amino-6-bromobenzenethiol

Chemical Property of 2-Amino-6-bromobenzenethiol

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Amino-6-bromobenzenethiol

There total 1 articles about 2-Amino-6-bromobenzenethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-6-bromobenzothiazole (15864-32-1) → 2-amino-5-bromobenzenethiol (824932-42-5)

Guidance literature:

2-amino-6-bromobenzothiazole; With potassium hydroxide; water; Heating / reflux;

With water; acetic acid; at 20 ℃;

Reference yield: 82.5%

acetic anhydride (108-24-7) + 2-amino-5-bromobenzenethiol (824932-42-5) → 2-amino-5-bromothio-acetoxybenzene

Guidance literature:

With pyridine; aluminum oxide; at 82 - 85 ℃; for 2h; microwave irradiation;

DOI:10.1016/S0040-4039(02)00732-3

Reference yield: 69.0%

benzoic acid (65-85-0,8013-63-6) + 2-amino-5-bromobenzenethiol (824932-42-5) → 7-bromo-2-phenylbenzo[d]thiazole (36247-07-1)

Guidance literature:

With polyphosphoric acid; at 160 ℃; for 6h;

upstream raw materials:

2-amino-6-bromobenzothiazole

Downstream raw materials:

5-[4-(6-bromo-1,3-benzothiazol-2-yl)phenyl]-1,3-oxazole

7-bromo-2-phenylbenzo[d]thiazole

Refernces