2-Iodo-4,6-dinitrotoluene

Base Information

Chemical Name:2-Iodo-4,6-dinitrotoluene
CAS No.:29270-49-3
Molecular Formula:C7H5IN2O4
Molecular Weight:308.03
Hs Code.:2904909090
DSSTox Substance ID:DTXSID50477743
Wikidata:Q82310633
Mol file:29270-49-3.mol

Synonyms:2-Iodo-4,6-dinitrotoluene;29270-49-3;1-iodo-2-methyl-3,5-dinitrobenzene;Benzene, 1-iodo-2-methyl-3,5-dinitro-;DTXSID50477743

Suppliers and Price of 2-Iodo-4,6-dinitrotoluene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-IODO-4,6-DINITROTOLUENE 95.00%
5MG
$ 498.04

Total 4 raw suppliers

Chemical Property of 2-Iodo-4,6-dinitrotoluene

Chemical Property:

PSA：91.64000
LogP:3.46240
XLogP3:2.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:307.92940
Heavy Atom Count:14
Complexity:249

Purity/Quality:

99% ^*data from raw suppliers

2-IODO-4,6-DINITROTOLUENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=C(C=C1I)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 2-Iodo-4,6-dinitrotoluene

There total 2 articles about 2-Iodo-4,6-dinitrotoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 121-14-2
2,4-dinitrotoluene

: 29270-49-3
2-iodo-4,6-dinitrotoluene

Guidance literature:: With reagent "I⁽¹⁺⁾"; In sulfuric acid; at 100 ℃; for 6.5h;
DOI:10.1007/BF02495292

Reference yield:

: 7745-92-8
2-iodo-1-methyl-4-nitrobenzene

: 29270-49-3
2-iodo-4,6-dinitrotoluene

Guidance literature:: With sulfuric acid; nitric acid;
DOI:10.1021/jo01076a601

Reference yield:

: 29270-49-3
2-iodo-4,6-dinitrotoluene

: 36994-79-3
2,4,6-triiodo-toluene

Guidance literature:: Multi-step reaction with 4 steps

1: H₂S, aq. NH₃ / dioxane

2: (i) NaNO₂, H₃PO₄, H₂SO₄, (ii) KI

3: Sn, aq. HCl

4: (i) NaNO₂, H₃PO₄, H₂SO₄, (ii) KI

With hydrogenchloride; ammonium hydroxide; tin; hydrogen sulfide; In 1,4-dioxane;
DOI:10.1039/j39700001480